Preparation method of oxidation modified cb/cfdsf/ag-80 epoxy resin composite

A technology of AG-80 and epoxy resin, which is applied in the fields of dry-cleaning fiber products, fiber treatment, textiles and papermaking, etc., can solve problems such as insufficient mechanical properties such as strength, affecting the performance of composite material matrix, and affecting the physical properties of composite material systems. To achieve the effect of ensuring stability and good electrical conductivity

Active Publication Date: 2020-06-23
SHAANXI SCI TECH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0014] Chinese patent application (201310413596.3) discloses a modified carbon fiber / epoxy resin composite material and a preparation method thereof. The preparation method includes the steps of mixing graphene with liquid epoxy resin to obtain a first mixture. In the first mixture Add a curing agent capable of cross-linking and curing the liquid epoxy resin to obtain the second mixture, and use the carbon fiber and the second mixture as raw materials to make the liquid epoxy resin cross-link and cure to form a modified compound integrated with the carbon fiber. The carbon fiber / epoxy resin composite material has a simple process and high production efficiency, but its strength and other mechanical properties are insufficient
[0015] From the above literature, it is easy to know that the difference in the type and content of CB will greatly affect the performance of the composite material matrix, and then have a great impact on the physical properties of the composite material system.

Method used

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  • Preparation method of oxidation modified cb/cfdsf/ag-80 epoxy resin composite
  • Preparation method of oxidation modified cb/cfdsf/ag-80 epoxy resin composite
  • Preparation method of oxidation modified cb/cfdsf/ag-80 epoxy resin composite

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Embodiment 1

[0041] For the modification treatment of carbon black (CB), the inventor of the present application has studied the use of silane coupling agent to carry out modification treatment and the use of oxidant to carry out modification treatment. The protection of the present invention adopts oxidation modification CB / CFDSF / AG-80 The preparation method of oxygen resin composite material;

[0042] A preparation method for preparing oxidation-modified CB / CFDSF / AG-80 epoxy resin composite material, mainly comprising the following steps:

[0043] 1. Modification of carbon black (CB) with concentrated nitric acid

[0044] Use concentrated nitric acid to modify carbon black (CB). First, take 4g of carbon black and 50ml of concentrated nitric acid with a concentration of 65wt% and pour them into a beaker, heat to 100°C and stir for 2 hours, then dilute with distilled water and filter with suction , scrape off the filtered CB carefully, put it into a beaker and pour a large amount of disti...

Embodiment 2

[0051] Modification of carbon black (CB) The inventor of the present application has studied the use of silane coupling agent for modification and the use of oxidant for modification. The protection of the present invention uses oxidation modified CB / CFDSF / AG-80 epoxy The preparation method of resin composite material;

[0052] A preparation method for preparing oxidation-modified CB / CFDSF / AG-80 epoxy resin composite material, mainly comprising the following steps:

[0053] 1. Modification of carbon black (CB) with concentrated nitric acid

[0054] Carbon black (CB) is modified with concentrated nitric acid. Take 8g of carbon black and 75ml of concentrated nitric acid with a concentration of 68wt% and pour them into a beaker, heat to 100°C and stir for 2.5 hours, then dilute with distilled water and filter with suction , scrape off the filtered CB carefully, put it into a beaker and pour a large amount of distilled water to continue to dilute, after standing for a proper time...

Embodiment 3

[0061] Modification of carbon black (CB) The inventor of the present application has studied the use of silane coupling agent for modification and the use of oxidant for modification. The protection of the present invention uses oxidation modified CB / CFDSF / AG-80 epoxy The preparation method of resin composite material;

[0062] A preparation method for preparing oxidation-modified CB / CFDSF / AG-80 epoxy resin composite material, mainly comprising the following steps:

[0063] 1. Modification of carbon black (CB) with concentrated nitric acid

[0064] Carbon black (CB) is modified with concentrated nitric acid, 12g of carbon black and 100ml of concentrated nitric acid with a concentration of 70wt% are poured into a beaker, heated to 110°C and fully stirred for 3 hours, then diluted with distilled water and suction filtered. Carefully scrape off the filtered CB, put it into a beaker and pour a large amount of distilled water to continue diluting. After standing for an appropriate...

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Abstract

The invention relates to a preparation method for an oxidation modified CB / CFDSF / AG-80 epoxy resin composite material. The preparation method mainly comprises the following steps: step 1, modificationtreatment of carbon black with concentrated nitric acid; step 2, surface cleaning and surface modification treatment of carbon fiber double-layer spaced fabric (CFDSF); and step 3, pouring and thermocuring of CFDSF with a prepared modified CB / AG-80 epoxy resin solution. According to the invention, the concentrated nitric acid modified CB / CFDSF / AG-80 epoxy resin composite material prepared throughthe above-mentioned preparation steps and concrete process parameters thereof and with advantages of good conductivity, thermodynamic properties and less usage amount of a conducting material has thefollowing advantages: modified carbon black is uniformly distributed in a matrix; and the composite material has good conductive stability and can be extensively applied to the fields of electronics,electrostatic protection, electromagnetic shielding, microwave absorption, etc.

Description

technical field [0001] The invention relates to the field of composite materials, in particular to an oxidation-modified CB / CFDSF (carbon fiber double-layer spacer fabric) / AG-80 epoxy resin composite material and a preparation method thereof. Background technique [0002] With the rapid development of the electronic technology industry, the demand for functional composite materials with good electrical conductivity is also increasing. Since the conductive composite material has the characteristics of light weight, no rust, good dimensional stability, and adjustable conductivity in a wide range, it is also easy to process into various complex shapes and easy to mass industrial production, so it is used in electrostatic protection. , electromagnetic shielding, microwave absorption and other fields are widely used. At present, the common conductive composite materials usually use polymer as the matrix, and at the same time add conductive substances such as carbon-based materia...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08G59/42C08G59/68C08K9/02C08K3/04C08K9/06C08K7/00C08K7/06D06L1/02D06M13/513D06M101/40
CPCC08G59/4223C08G59/686C08K3/04C08K7/00C08K7/06C08K9/02C08K9/06C08K2201/001D06L1/02D06M13/513D06M2101/40
Inventor 李亚鹏邵媛媛张鹏飞付骋宇蓝海啸
Owner SHAANXI SCI TECH UNIV
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