Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

41results about How to "Good surface modification" patented technology

Surface modification method for nano calcium carbonate

The invention discloses a surface modification method for nano calcium carbonate, which is characterized by comprising the following steps of: adding inorganic alkali into nano calcium carbonate slurry, uniformly stirring, heating the slurry, adding fatty acid and performing surface modification. The method comprises the following specific steps of: adding a certain amount of nano calcium carbonate slurry into a reaction kettle, adding 0.00004 to 0.00040mol of inorganic alkali into 1g of CaCO3, and uniformly stirring; heating to the temperature of between 75.0 and 90.0 DEG C, adding 0.00005 to 0.00035mol of fatty acid or fatty acid salt into 1g of nano calcium carbonate (CaCO3) slurry, reacting, and continuously stirring for 30 to 120 minutes; and after surface modification reaction is finished, cooling, filtering, washing, drying and grinding the slurry to obtain the nano calcium carbonate subjected to surface modification. The method is simple and practicable, a modifier can form a uniform and complete coating layer on the surface of the nano calcium carbonate, and the modified product has a good application effect in polymer such as silicone sealant, polyvinyl chloride (PVC) paste resin and the like.
Owner:GUANGXI HUANA NEW MATERIALS TECH CO LTD

Surface treatment method of nano-calcium carbonate used for polyvinyl chloride plastisol

The invention discloses a surface treatment method of nano-calcium carbonate used for polyvinyl chloride plastisol. The surface treatment method comprises the following steps: adding nano-calcium carbonate serous fluid into a reaction kettle, wherein the specific surface area (BET) of nano-calcium carbonate in the serous fluid is 18.0-60.0m<2> / g and the pH of the nano-calcium carbonate serous fluid is 8.5-9.5; heating to 70-95 DEG C, stirring, adding a mixed modifier accounting for 1.8-6.0% of the mass of the nano-calcium carbonate in the serous fluid, continuing stirring for 30-180 minutes, thus completing surface treatment. The mixed modifier is a mixture of stearic acid alkali metal saponified matter and calcium stearate, the mass ratio of fatty acid to calcium stearate in the complex modifier is 20-70%, and the proportion of the using quantity of the fatty acid to a saponifier is 1: 1. According to the method, the fatty acid is saponified by a strong base, so that the shortcoming that the fatty acid is difficult to react with the surface of calcium carbonate in water to generate the calcium stearate during wet process surface modification of the nano-calcium carbonate can be overcome; and the calcium stearate is directly introduced through fatty acid saponification liquor, so that a significant surface modification effect is obtained. The method has the advantages that raw materials are low in price and easy to obtain, the processes are simple and feasible, and the quality of a product is state. The method has significant economic benefits and social benefits.
Owner:GUANGXI HUANA NEW MATERIALS TECH CO LTD

Co-extrusion formed wood-plastic composite plate and preparation method thereof

The invention discloses a co-extrusion formed wood-plastic composite plate and a preparation method thereof, which discloses a composite material, a structural material and the preparation method of the materials. The co-extrusion formed wood-plastic composite plate is composed of an anti-aging resin layer and a wood-plastic structural layer, wherein the anti-aging resin layer is located on the surface of the wood-plastic structural layer. The anti-aging resin layer is formed by melting, blending and extruding an ASA (Acrylonitile-Styrene-Acrylate) resin, titanium dioxide, an antioxidant and a light stabilizer; and the wood-plastic structural layer is formed by extruding polyethylene, wood power, calcium powder, a rare-earth coupling agent, chlorinated polyethylene, acrylic resin, polyethylene wax, octyl stearate and ethylene bis stearamide. Different molten material flows are formed by the anti-aging resin layer and the wood-plastic structural layer, and then the material flows are converged in a compound machine head and co-extruded by a neck mould, so that the co-extrusion formed wood-plastic composite plate is prepared. Besides the characteristics of multiple purposes of common wood-plastic plates, the wood-plastic plate has more excellent anti-aging property and does not age after a long use in the open air. The co-extrusion formed wood-plastic composite plate disclosed by the invention is suitable for preparing indoor and outdoor floors, guardrails, decorative sheets and the like.
Owner:NANJING FORESTRY UNIV

Epoxy resin-based well cementing fluid and preparation method thereof

The invention relates to an epoxy resin-based well cementing fluid and a preparation method thereof. The well cementing fluid includes, by weight, 100 parts of bisphenol A oily epoxy resin, 15-35 parts of an active diluent, 10-25 parts of a diluent, 10-20 parts of an aromatic amine curing agent, 0.1-5.0 parts of a curing accelerator, 0.1-3.0 parts of a flexibilizer, 0-210 parts of a density regulator, 0.1-5.0 parts of a suspension stabilizer and 1-3 parts of natural bamboo fibers. The flexibilizer is modified nano graphene oxide, and is prepared by the following steps: dissolving nano grapheneoxide powder into an ethanol solution; carrying out ultrasonic treatment to form a uniform dispersion liquid; adjusting the pH value of the system to 3-5; slowly dropwise adding an absolute ethyl alcohol mixed solution of gamma-aminopropyltriethoxysilane; putting the mixture into a microwave reactor for treatment; then performing washing, centrifugation, drying and grinding. The well cementing fluid is good in flowability, easy to pump, adjustable in thickening time, wide in density range and wide in applicable temperature, and the preparation method is reliable in principle, easy and convenient to operate and free of pollution to the environment and has wide market application prospects.
Owner:BC P INC CHINA NAT PETROLEUM CORP +2

Preparation method for silane coupling agent modified CNTs/CFDSF/AG-80 epoxy resin composite material

The invention relates to a preparation method for a silane coupling agent modified CNTs / CFDSF / AG-80 epoxy resin composite material. The preparation method mainly comprises the following steps: step 1,acidification of carbon nanotubes (CNTs) with a mixed acid solution of concentrated nitric acid and concentrated sulfuric acid; step 2, modification of O-CNTs obtained by acidification treatment through a silane coupling agent; step 3, surface cleaning and surface modification treatment of carbon fiber double-layer spaced fabric (CFDSF); and step 4, pouring and thermocuring of CFDSF with a prepared modified CNTs / AG-80 epoxy resin solution. According to the invention, the silane coupling agent modified CNTs / CFDSF / AG-80 epoxy resin composite material prepared through the above-mentioned preparation steps and concrete process parameters thereof and with advantages of good conductivity, thermodynamic properties and less usage amount of a conducting material has the following advantages: modified carbon nanotubes are uniformly distributed in a matrix; and the composite material has good conductive stability and can be extensively applied to the fields of electronics, electrostatic protection, electromagnetic shielding, microwave absorption, etc.
Owner:SHAANXI SCI TECH UNIV

Silicate-modified PVC foamed composite decorative sheet and manufacturing method thereof

The invention discloses a silicate-modified PVC foamed composite decorative sheet and a manufacturing method thereof. The manufacturing method is mainly used for manufacturing a decorative sheet used in occasions such as a family, an office, a shopping mall and a meeting, and belongs to the technical field of composite materials. The silicate-modified PVC foamed composite decorative sheet mainly comprises three layers, namely a decorative layer, a foaming layer and a supporting layer, wherein the supporting layer is mainly prepared from silicate inorganic filler, polyvinyl chloride and a processing aid; the foaming layer is mainly prepared from silicate inorganic filler, polyvinyl chloride, a foaming agent and a processing aid; the decorative layer is mainly prepared from silicate inorganic filler, polyvinyl chloride, a color masterbatch and a processing aid. The decorative sheet has the advantages of being free of toxicity and odor as well as formaldehyde, being capable of preventing water, dampness, worm damage, light mass and high surface decoration property, being nailable, sawable and planeable, being capable of reducing the consumption of wood and macromolecular polymers, and being relatively high in strength and relatively long in service life.
Owner:SICHUAN MIANNING XICHENG TALC MINING

Real silk aluminum foil composite steel plate and manufacturing method thereof

The invention provides a real silk aluminum foil composite steel plate and a manufacturing method thereof. The composite steel plate comprises a PE (polyethylene) protection film, a PET (polyethylene glycol terephthalate) real silk film, a steel plate and a back coating layer which are arranged in sequence from top to bottom and are closely connected with one another. The manufacturing method comprises the following steps of pre-degreasing the steel plate, degreasing and washing by water, coating the back surface of the steel plate with an epoxy resin coating by rolling, solidifying and drying to form the back coating layer, coating the bottom coating layer of the steel plate with a polyurethane adhesive, solidifying to form a second adhesive layer, and compounding the second adhesive layer with a real silk aluminum foil film to obtain the real silk aluminum foil composite steel plate. Compared with a general composite steel plate, the real silk aluminum foil composite steel plate manufactured by adopting the method is better in metal luster and surface modification property, relatively low in relative cost, excellent in performance and environment-friendly in manufacturing process, and especially is very popular in consumers due to the characteristic of diversified appearances; the technical gap in the field of real silk aluminum foil composite steel plates in China is filled up.
Owner:合肥禾盛新型材料有限公司

Surface modification method for nano calcium carbonate

The invention discloses a surface modification method for nano calcium carbonate, which is characterized by comprising the following steps of: adding inorganic alkali into nano calcium carbonate slurry, uniformly stirring, heating the slurry, adding fatty acid and performing surface modification. The method comprises the following specific steps of: adding a certain amount of nano calcium carbonate slurry into a reaction kettle, adding 0.00004 to 0.00040mol of inorganic alkali into 1g of CaCO3, and uniformly stirring; heating to the temperature of between 75.0 and 90.0 DEG C, adding 0.00005 to 0.00035mol of fatty acid or fatty acid salt into 1g of nano calcium carbonate (CaCO3) slurry, reacting, and continuously stirring for 30 to 120 minutes; and after surface modification reaction is finished, cooling, filtering, washing, drying and grinding the slurry to obtain the nano calcium carbonate subjected to surface modification. The method is simple and practicable, a modifier can form a uniform and complete coating layer on the surface of the nano calcium carbonate, and the modified product has a good application effect in polymer such as silicone sealant, polyvinyl chloride (PVC) paste resin and the like.
Owner:GUANGXI HUANA NEW MATERIALS TECH CO LTD

Ultralow-temperature rolling imprinting strengthening method and device for surface of austenitic stainless steel plate

The invention provides an austenitic stainless steel plate surface ultralow-temperature rolling imprinting strengthening method and device, and belongs to the technical field of special steel surface modification. The invention provides an austenitic stainless steel plate surface ultralow-temperature rolling impressing strengthening method and device aiming at the defects that when an austenitic stainless steel plate is in service, the surface hardness is low, scratching is prone to occurring, and attractiveness is affected. Firstly, a stainless steel plate is placed on a supporting plate in a cooling tank to be positioned, the positioned stainless steel plate and a corrugated roller are soaked and cooled at the same time through an ultralow-temperature medium filled in the cooling tank, and the temperature of the stainless steel plate is kept at the liquid nitrogen temperature. The cooled corrugated roller is driven by the servo hydraulic system to conduct rolling coining on the upper surface and the lower surface of the stainless steel plate in the liquid nitrogen environment, so that the surface strength and hardness of the stainless steel plate are remarkably improved. The austenitic stainless steel plate surface ultralow-temperature rolling imprinting strengthening method and device have the advantages of being rapid, efficient, environmentally friendly, remarkable in process integration level and strengthening effect and the like.
Owner:XINJIANG UNIVERSITY

Surface treatment method of nano-calcium carbonate used for polyvinyl chloride plastisol

The invention discloses a surface treatment method of nano-calcium carbonate used for polyvinyl chloride plastisol. The surface treatment method comprises the following steps: adding nano-calcium carbonate serous fluid into a reaction kettle, wherein the specific surface area (BET) of nano-calcium carbonate in the serous fluid is 18.0-60.0m<2> / g and the pH of the nano-calcium carbonate serous fluid is 8.5-9.5; heating to 70-95 DEG C, stirring, adding a mixed modifier accounting for 1.8-6.0% of the mass of the nano-calcium carbonate in the serous fluid, continuing stirring for 30-180 minutes, thus completing surface treatment. The mixed modifier is a mixture of stearic acid alkali metal saponified matter and calcium stearate, the mass ratio of fatty acid to calcium stearate in the complex modifier is 20-70%, and the proportion of the using quantity of the fatty acid to a saponifier is 1: 1. According to the method, the fatty acid is saponified by a strong base, so that the shortcoming that the fatty acid is difficult to react with the surface of calcium carbonate in water to generate the calcium stearate during wet process surface modification of the nano-calcium carbonate can be overcome; and the calcium stearate is directly introduced through fatty acid saponification liquor, so that a significant surface modification effect is obtained. The method has the advantages that raw materials are low in price and easy to obtain, the processes are simple and feasible, and the quality of a product is state. The method has significant economic benefits and social benefits.
Owner:GUANGXI HUANA NEW MATERIALS TECH CO LTD

a tic-cr 7 c 3 -cnts/iron-based surface composite material and preparation method thereof

The invention discloses a composite material belonging to the field of surface engineering, and in particular relates to a TiC-Cr7C3-CNTs / iron based surface composite material and a preparation method thereof. The preparation method comprises the following steps: pretreating an Fe-Cr-Ni stainless steel material, then reacting for 18-22 hours in a 680-700 DEG C supersaturated carbon atmosphere containing 68% of CO, 31% of H2 and 1% of H2O to obtain uniformly distributed CNTs on the surface of the stainless steel, and weighing the stainless steel before and after the reaction to obtain a difference value namely the weight of increased carbon; and according to the weight of the increased carbon, weighing Ti powder and Ni powder, mixing the Ti powder and Ni powder, and preparing the TiC-Cr7C3-CNTs / iron based surface composite material by adopting a laser cladding synchronous powder feeding technology. The composite material prepared by the method disclosed by the invention has strong cohesive force with the surface of a metal matrix, is difficult to fall off, and is high in hardness and excellent in acid corrosion resistance. The composite material disclosed by the invention has an extremely significant effect on modifying the surface of a steel and iron material, and expands the application field of steel and iron.
Owner:SHANGHAI MARITIME UNIVERSITY

Nano-graphite sol preparation device and method

The invention relates to the field of nano-graphite sol preparation and discloses a nano-graphite sol preparation device. The device comprises an electrolytic cell, flushing pipes and limiting cover plates, wherein the electrolytic cell comprises a cell body, a plurality of graphite supports are arranged at intervals in the width direction of the cell body, a plurality of groups of one-to-one corresponding support opening grooves are formed between every two adjacent graphite supports, a graphite plate is arranged between every group of support opening grooves, and one pair of diagonal cornersof each graphite plate are supported in the corresponding group of support opening grooves; the limiting cover plates are strip-shaped, a plurality of clamping grooves are formed in bottom surfaces of the limiting cover plates at intervals in the length direction, the limiting cover plates are arranged above the graphite plates, and the graphite plates are separated by the clamping grooves one byone; the flushing pipes are arranged along inner side walls of the cell body and extend along the bottom surface of the cell body. The invention further discloses a preparation method. The problem that the nano-graphite sol is easy to agglomerate in the preparation process can be solved, and the nano-graphite sol consumes short time during preparation and has few impurity ions, small particle size, high concentration and good stability.
Owner:曹明辉
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products