Filler-containing pressure-sensitive adhesive tape and method of producing filler-containing pressure-sensitive adhesive tape
A pressure-sensitive adhesive and pressure-sensitive adhesive layer technology, which is used in the manufacture of filler-containing pressure-sensitive adhesive tapes and filler-containing pressure-sensitive adhesive tapes, can solve uneven heat spread, reduce pressure-sensitive adhesive Mixture layer, difficulties and other problems, to achieve excellent pressure-sensitive adhesive force, the effect of inhibiting the generation of volatile components
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Embodiment 1
[0181] (Manufacture of slurry composition A)
[0182]Liquid monomer mixture (monomer composition) obtained by mixing 84 parts by mass of 2-ethylhexyl acrylate (2EHA) and 16 parts by mass of N-vinyl-2-pyrrolidone (NVP) as monomer components With 0.05 parts by mass of a photopolymerization initiator available under the trade name "IRGACURE 651 (2,2-dimethoxy-1,2-diphenylethan-1-one)" (manufactured by BASF Japan Ltd.) It was blended with 0.05 parts by mass of a photopolymerization initiator available under the trade name "IRGACURE 184 (1-hydroxycyclohexyl phenyl ketone)" (manufactured by BASF Japan Ltd.). After that, the resultant was irradiated with ultraviolet light until its viscosity (Viscometer: manufactured by TOKIMEC, VISCOMETER (model: BH)) became about 6.4 Pa·s. Thus, a syrupy composition A (2EHA / NVP=84 / 16) containing a partial polymer (prepolymer) obtained by polymerizing a part of the monomer components by irradiation was obtained.
[0183] (Manufacture of pressure s...
Embodiment 2
[0191] The pressure-sensitive adhesive tape of Example 2 (thickness of the pressure-sensitive adhesive layer: 50 μm) was produced in the same manner as in Example 1 except that the blending amount of acrylic acid (AA) was changed to 5 parts by mass.
Embodiment 3
[0193] The pressure-sensitive adhesive tape of Example 3 (thickness of the pressure-sensitive adhesive layer: 50 μm) was produced in the same manner as in Example 1 except that the blending amount of acrylic acid (AA) was changed to 10 parts by mass.
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