A kind of preparation method and application of metal-polyphenol nanoparticles
A nanoparticle and metal technology, applied in the field of nanoparticle preparation, can solve the problems of decreased photothermal treatment effect, weakened EPR effect, shortened cycle time, etc., and achieve good biodegradability, good absorption, and cheap raw materials.
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Embodiment 1
[0021] A preparation method of metal-polyphenol nanoparticles, comprising the steps of:
[0022] 1) Weigh 2.5 g of tannic acid and dissolve in 70 mL of distilled water, and dissolve 0.1 g of ammonium metavanadate in 30 mL of distilled water, and stir them evenly for later use;
[0023] 2) Heat the ammonium metavanadate solution to 60°C and stir for 60 min to obtain a golden yellow solution, namely the vanadium oxide solution;
[0024] 3) After adding the vanadium oxide solution dropwise to the tannic acid solution, react at 60°C for 24 h to obtain a black solution;
[0025] 4) Dialyze the black solution obtained in the previous step, change the distilled water every 2-3 hours for the first 12 hours, and change the distilled water every 5-6 hours for the next 36 hours to obtain the final product.
[0026] 5) The storage temperature of the final product is 4°C.
Embodiment 2
[0028] A preparation method of metal-polyphenol nanoparticles, comprising the steps of:
[0029] 1) Weigh 2.5 g of tannic acid and dissolve in 70 mL of distilled water, and dissolve 0.1 g of ammonium metavanadate in 30 mL of distilled water, and stir them evenly for later use;
[0030] 2) Heat the ammonium metavanadate solution to 80°C and stir for 30 minutes to obtain a golden yellow solution, namely the vanadium oxide solution;
[0031] 3) After adding the vanadium oxide solution dropwise to the tannic acid solution, react at 80°C for 24 h to obtain a black solution;
[0032] 4) Dialyze the black solution obtained in the previous step, change the distilled water every 2-3 hours for the first 12 hours, and change the distilled water every 5-6 hours for the next 36 hours to obtain the final product.
[0033] 5) The storage temperature of the final product is 4°C.
Embodiment 3
[0035] A preparation method of metal-polyphenol nanoparticles, comprising the steps of:
[0036] 1) Weigh 2.5 g of tannic acid and dissolve in 70 mL of distilled water, and dissolve 0.1 g of ammonium metavanadate in 30 mL of distilled water, and stir them evenly for later use;
[0037] 2) Heat the ammonium metavanadate solution to 100°C and stir for 10 minutes to obtain a golden yellow solution, namely the vanadium oxide solution;
[0038] 3) After adding the vanadium oxide solution to the tannic acid solution dropwise, react at 100°C for 24 h to obtain a black solution;
[0039] 4) Dialyze the black solution obtained in the previous step, change the distilled water every 2-3 hours for the first 12 hours, and change the distilled water every 5-6 hours for the next 36 hours to obtain the final product.
[0040] 5) The storage temperature of the final product is 4°C.
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