A kind of low-temperature heat-sealing dispersion liquid and preparation method thereof
A low-temperature heat-sealing and dispersion technology, applied in the direction of coating, etc., can solve the problems of increased scrap rate, low heat-sealing temperature, and inability to fully meet the packaging needs of first-use
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Embodiment 1
[0018] 25% sarin resin
[0019] 2% acrylic resin
[0020] 1.4% compound emulsifier
[0021] 0.1% defoamer
[0022] 1.5% pH regulator
[0023] 70% deionized water.
[0024] 1) Configuration of compound emulsifier
[0025] Weigh 2.1g of propylene glycol monolaurate and 0.7g of alkyl sulfate compound emulsifier and mix with 14g of deionized water, heat to 50°C, stir while heating at a stirring speed of 70 rpm, stir for 1h, and set aside .
[0026] 2) Preparation of dispersion
[0027] Add 126g of deionized water, 50g of sarin resin and 4g of acrylic resin into the reaction kettle, stir at a stirring speed of 200 rpm, add the prepared compound emulsifier, and replace it by vacuuming→adding nitrogen for 3 Finally, fill in nitrogen to make the pressure in the kettle reach 1Mpa, adjust the stirring speed to 2000 rpm, heat to 90°C, keep the temperature at a constant temperature for 3 hours, add 0.2g defoamer and 3g pH regulator again, stir fully, and the stirring speed is 100 ...
Embodiment 2
[0030] 24% sarin resin
[0031] 2% acrylic resin
[0032] 1% compound emulsifier
[0033] 0.2% defoamer
[0034] 1.5% pH regulator
[0035] 71.3% deionized water.
[0036] 1) Configuration of compound emulsifier
[0037] Weigh 2.4g of propylene glycol monolaurate and 0.6g of alkyl sulfate compound emulsifier and mix with 21.4g of deionized water, heat to 52°C, stir while heating, the stirring speed is 80 rpm, stir for 1h, wait use.
[0038] 2) Preparation of dispersion
[0039] Add 192.5g of deionized water, 72g of sarin resin and 6g of acrylic resin into the reaction kettle, stir at a stirring speed of 300 rpm, add the prepared compound emulsifier, and replace by vacuuming→adding nitrogen 3 times, finally fill in nitrogen to make the pressure inside the kettle reach 1Mpa, adjust the stirring speed to 2000 rpm, heat to 91°C, keep the temperature constant for 4 hours, add 0.6g defoamer, 4.5g pH regulator again, stir fully, stir The speed is 110 rpm, and after cooling do...
Embodiment 3
[0042] 22% sarin resin
[0043] 3% acrylic resin
[0044] 3% compound emulsifier
[0045] 0.1% defoamer
[0046] 1.5% pH regulator
[0047] 70.4% deionized water.
[0048] 1) Configuration of compound emulsifier
[0049] Weigh 18g of propylene glycol monolaurate, 6g of alkyl sulfate compound emulsifier and 56.3g of deionized water and mix them, heat to 51°C, stir while heating at a stirring speed of 90 rpm, stir for 1h, and set aside.
[0050] 2) Preparation of dispersion
[0051] Add 506.9g of deionized water, 176g of sarin resin and 24g of acrylic resin into the reaction kettle, stir at a stirring speed of 300 rpm, add the prepared compound emulsifier, and replace by vacuuming→adding nitrogen 3 times, and finally filled with nitrogen to make the pressure in the kettle reach 1Mpa, adjust the stirring speed to 2000 rpm, heat to 92°C, keep the temperature for 4 hours, add 0.8g defoamer, 12g pH regulator again, stir fully, the stirring speed 120 rev / min, after cooling dow...
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