Coolant
A technology of cold storage agent and auxiliary agent, applied in the field of cold storage agent, can solve the problems of narrow phase transition temperature range, small water absorption, slow water absorption speed, etc., and achieve the effect of improving the phase transition temperature range, fast water absorption speed and reversible process.
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[0030] The preparation method of super absorbent resin comprises the following steps:
[0031] (1) Take distiller's grains and crush them through a 100-mesh sieve. Take the sieved particles and mix them with catalyst and sodium carbonate according to the mass ratio of 20~25:1:3~6. Let stand for 1~2h, filter, and take the filter residue in an oven at 60~80°C After drying, move to the container and crack at 600-800°C for 4-7 hours at high temperature in a muffle furnace to obtain cracked slag. Take the cracked slag, add 25-35% of the cracked slag mass to infiltrate it, and paste it with 300W ultrasonic paste at 50-70°C. Melt for 5-10 minutes to get gelatinized product;
[0032] (2) In an ice-water bath, take acrylic acid at a mass ratio of 1:3~6 and add KOH solution with a mass fraction of 25~30% to mix, and stir at 220~260r / min for 30~45min to obtain a neutralizing solution, and add the gelatinized product Initiator with 3-6% gelatin mass, cross-linking agent with 4-8% gelatin...
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