A method for measuring the agglomeration degree of ferromagnetic powder in a suspension system

A measurement method, ferromagnetic technology, applied in the direction of nuclear magnetic resonance analysis, etc., can solve the problem of difficult comparison of dispersion effect, achieve the effect of improving production process and product performance, simple process and good repeatability

Inactive Publication Date: 2021-03-26
SHANGHAI UNIV OF MEDICINE & HEALTH SCI
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Problems solved by technology

[0009] The present invention aims to solve the problems existing in the prior art, and provides a method for measuring the agglomeration degree of ferromagnetic powder in a water-based suspension system. The nuclear magnetic resonance technology is used to measure the agglomeration degree of ferromagnetic powder in the suspension system, which is used to solve the problem of powder materials in the suspension system. It is difficult to compare the dispersion effect under different aqueous solution environments and different concentrations, so as to achieve the purpose of scientifically evaluating the state of powder agglomeration

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  • A method for measuring the agglomeration degree of ferromagnetic powder in a suspension system

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Embodiment

[0039] Method for determining the degree of ferromagnetic powder in a suspension system, including the following steps:

[0040] (1) The powder suspension solution of different solid content ω, the solute is ferromagnetic powder, the solvent is water;

[0041] (2) The solution prepared by the step (1) is separately diluted with pure water, and then the nucleate is measured by the nuclear magnetic resonance technique, respectively, and the Tricho Sample of different gradient concentration powder after the dilution is used. 2 Relaxation time and calculate the relaxation rate R 2 R 2f Where R 2 R 2f The relaxation rate of the powder particulate suspension system and the solvent, that is, respectively, respectively. 2 The reciprocal of the relaxation time; the powder suspension solution that finally derived different solid content is completely dispersed at the Ω 'value of the powder in completely dispersed, and Ω' is completely dispersed in the ideal state;

[0042] (3) Calculate the...

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Abstract

The invention discloses a determination method for an agglomeration degree of ferromagnetism powder in a suspension system. The determination method comprises the following steps: (1) preparing different solid contents omega of powder suspension solutions; (2) utilizing pure water to respectively and serially dilute the solutions, then utilizing a nuclear magnetic resonance technology for respectively measuring T2 relaxation time of the pure water and T2 relaxation time of the different gradient concentrations of diluted powder suspension solution samples and calculating out relaxation rates R2 and R2f; (3) calculating out the agglomeration degree phi (%) of powder in the suspension system; (4) drawing a corresponding relation curve between the agglomeration degrees phi (%) of the powder materials and the powder materials under different solid contents omega in the system and using the corresponding relation curve to evaluate dispersity difference of the powder materials. The determination method disclosed by the invention is simple and practical to operate, can effectively evaluate dispersity difference of powder particles in the suspension system, achieves the purpose of scientifically representing the agglomeration degrees of the powder materials and is favorable for improving powder material production technologies and product performance.

Description

Technical field [0001] The present invention relates to a method of determining the degree of ferromagnetic powder in a suspension system, and more particularly to a method for determining the ferromagnetic powder in a suspension system using nuclear magnetic resonance techniques. Background technique [0002] The basic particle size is in submicron, and the nanometer powder material gives the above material special properties due to small dimensional effects, surface effects, quantum dimensional effects, or macro quantum tunneling effects. Scientifically characterize the aggregation state of the above powder material (degree of agglomeration), establishing an accurate description of the aggregation parameters of its structure, is of great significance for its application in the fields of medical, materials, biology, environment, manufacturing, energy, food and other fields. [0003] Taking nanomaterials as an example, due to its small size, the specific surface area is large, th...

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N24/08
CPCG01N24/08
Inventor 黄钢杨培强杨翼
Owner SHANGHAI UNIV OF MEDICINE & HEALTH SCI
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