The invention relates to a preparation process of grilled fish. The preparation method comprises the following steps of A, taking fresh and alive fish as raw material fish, and requiring no dead fish,diseased fish and deformed fish; B, removing scales of the raw material fish, wherein the raw material fish is cut into two halves from the back broken head to the fish tail, viscera, gills and blackmembranes in the abdomen are removed, and the surface of the raw material fish is cleaned and cut; C, preparing liquid medicine from a food additive, salt and water, putting spices into the liquid medicine, putting the raw material fish into the liquid medicine, performing static soaking for at least 2 hours, and controlling the static soaking temperature to be 9-11 DEG C; D, taking out the fish,controlling water, and uniformly smearing the front and back surfaces of the fish body with grilled fish marinade; E, enabling one fish to be put into one bag correspondingly, wherein the bag is sealed through a sealing machine, and a grilled fish product is obtained; and F, quickly freezing and cooling the grilled fish product, and storing the grilled fish product in an environment of minus 18 DEG C. The grilled fish product prepared by the method is free of fishy smell, natural in fragrance and tender and smooth in meat quality.