Device for repairing soil heavy mental pollution
A pollution remediation and heavy metal technology, applied in the restoration of polluted soil, water pollutants, water/sewage treatment, etc., can solve the problems of high manufacturing cost, convenient treatment of polluted water unfavorable to heavy metals, complex structure, etc.
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Embodiment 1
[0067] According to the following steps to prepare the catalase network 8-6 of the present invention, and in parts by weight:
[0068] Step 1: In the multi-tank reactor, add 341.0 parts of distilled water and 133.3 parts of 3-methylundecanonitrile, start the mixer in the multi-tank reactor, set the speed at 134rpm, and start the steam seal in the multi-tank reactor Steam heat exchanger, raise the temperature to 149.0°C, add 2-methoxy-5-methyl-4-[(4-methyl-2-nitrophenyl)azo]benzenediazo (T-4 ) Tetrachlorozincate (2:1) 136.2 parts, stirred evenly, reacted for 126.3 minutes, added 132.6 parts of ethyl 3-methylthiobutyrate, and the flow rate was 125.1m 3 / min of fluorine gas for 126.3 minutes; then add 135.2 parts of the golden leuco body in the multi-pot reactor, start the vapor-sealed steam heat exchanger in the multi-pot reactor again, raise the temperature to 166.2°C, keep it warm for 126.6 minutes, add 2,2'-[(1-methylethylene)bis[[2-(2-propenyl)-4,1-phenylene]oxymethylene]di...
Embodiment 2
[0074] According to the following steps to prepare the catalase network 8-6 of the present invention, and in parts by weight:
[0075] Step 1: In the multi-pot reactor, add 566.2 parts of distilled water and 175.5 parts of 3-methylundecanonitrile, start the mixer in the multi-pot reactor, set the speed at 180rpm, and start the steam seal in the multi-pot reactor Steam heat exchanger, raise the temperature to 150.2°C, add 2-methoxy-5-methyl-4-[(4-methyl-2-nitrophenyl)azo]benzenediazo (T-4 ) Tetrachlorozincate (2:1) 245.1 parts, stirred evenly, reacted for 137.5 minutes, added 149.7 parts of ethyl 3-methylthiobutyrate, and the flow rate was 166.7m 3 / min of fluorine gas for 137.5 minutes; then add 192.9 parts of golden leuco body into the multi-pot reactor, start the vapor seal steam heat exchanger in the multi-pot reactor again, raise the temperature to 199.1°C, keep it warm for 137.7 minutes, add 2,2'-[(1-methylethylene)bis[[2-(2-propenyl)-4,1-phenylene]oxymethylene]dioxirane...
Embodiment 3
[0081] According to the following steps to prepare the catalase network 8-6 of the present invention, and in parts by weight:
[0082] Step 1: In the multi-pot reactor, add 341.9 parts of distilled water and 133.9 parts of 3-methylundecanonitrile, start the mixer in the multi-pot reactor, set the speed at 134rpm, and start the steam seal in the multi-pot reactor Steam heat exchanger, raise the temperature to 149.9°C, add 2-methoxy-5-methyl-4-[(4-methyl-2-nitrophenyl)azo]benzenediazo (T-4 ) Tetrachlorozincate (2:1) 136.9 parts, stirred evenly, reacted for 126.9 minutes, added 132.9 parts of ethyl 3-methylthiobutyrate, and the flow rate was 125.9m 3 / min of fluorine gas for 126.9 minutes; then add 135.9 parts of golden leuco body into the multi-pot reactor, start the vapor seal steam heat exchanger in the multi-pot reactor again, raise the temperature to 166.9°C, keep it warm for 126.9 minutes, add 2,2'-[(1-methylethylene)bis[[2-(2-propenyl)-4,1-phenylene]oxymethylene]dioxirane...
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