Atmospheric treatment composite fiber filter material loaded with denitration catalyst, and preparation method
The technology of denitration catalyst and composite fiber is applied in the field of atmospheric control composite fiber filter material and preparation field loaded with denitration catalyst, which can solve the problems of low denitration efficiency, easy deactivation at high temperature, unstable properties, etc., and achieves high mechanical strength and adsorption capacity. , The effect of poor high temperature resistance and short service life
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Embodiment 1
[0029] (1) After blending polyimide fiber and polytetrafluoroethylene fiber, put it into the calcium hydroxide suspension prepared by mixing quicklime and water, take it out after ultrasonic treatment, and obtain the treated fiber filter material; polyimide The average fineness of amine fiber is 5 dtex, and the average length is 50mm; the average fineness of polytetrafluoroethylene fiber is 5 dtex, and the average length is 50mm; the ultrasonic frequency of ultrasonic treatment is 35kHz, and the ultrasonic treatment is 52min; in the preparation of fiber filter material, The mass ratio of water, quicklime, polyimide fiber and polytetrafluoroethylene fiber is 100:7:23:23;
[0030] (2) Dissolve cerium acetate, manganese nitrate, and ethanol in deionized water to prepare a mixed solution, add hydrogen peroxide with 8% mass of cerium acetate, then add the treated fiber filter material, and slowly add sodium silicate under heating and stirring conditions solution and reacted for 3 h...
Embodiment 2
[0035] (1) After blending polyimide fiber and polytetrafluoroethylene fiber, put it into the calcium hydroxide suspension prepared by mixing quicklime and water, take it out after ultrasonic treatment, and obtain the treated fiber filter material; polyimide The average fineness of amine fiber is 4dtex, and the average length is 30mm; the average fineness of polytetrafluoroethylene fiber is 3dtex, and the average length is 20mm; the ultrasonic frequency of ultrasonic treatment is 30kHz, and the ultrasonic treatment is 60min; in the preparation of fiber filter material, water , quicklime, polyimide fiber, polytetrafluoroethylene fiber mass ratio is 100:4:20:18;
[0036] (2) Dissolve cerium acetate, manganese nitrate, and ethanol in deionized water to prepare a mixed solution, add hydrogen peroxide with 8% mass of cerium acetate, then add the treated fiber filter material, and slowly add sodium silicate under heating and stirring conditions solution and reacted for 2 hours to obtai...
Embodiment 3
[0040] (1) After blending polyimide fiber and polytetrafluoroethylene fiber, put it into the calcium hydroxide suspension prepared by mixing quicklime and water, take it out after ultrasonic treatment, and obtain the treated fiber filter material; polyimide The average fineness of amine fiber is 8 dtex, and the average length is 70mm; the average fineness of polytetrafluoroethylene fiber is 6dtex, and the average length is 80mm; the ultrasonic frequency of ultrasonic treatment is 50kHz, and the ultrasonic treatment is 40min; in the preparation of fiber filter material, The mass ratio of water, quicklime, polyimide fiber and polytetrafluoroethylene fiber is 100: 8: 25: 26;
[0041] (2) Dissolve cerium acetate, manganese nitrate, and ethanol in deionized water to prepare a mixed solution, add hydrogen peroxide with 8% mass of cerium acetate, then add the treated fiber filter material, and slowly add sodium silicate under heating and stirring conditions solution and reacted for 5...
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