Resin dispersion liquid for waterborne two-component metallic paint and preparation method of resin dispersion liquid
A resin dispersion, water-based two-component technology, applied in the coating and other directions, can solve the problems of unstable metal powder, high price of metal powder, limited use, etc., to achieve the effect of good stability of finished products and low production cost
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[0039] The preparation method of above-mentioned water-based two-component metal paint resin dispersion liquid, comprises the steps:
[0040] (1) Add solvent and solvent gasoline into the reaction kettle according to the volume ratio (1~15): (1~20), and heat up to 100~140°C; (2) Methyl methacrylate, styrene, acrylic acid iso Octyl ester, hydroxyethyl methacrylate, acrylic acid, initiator according to volume ratio (20~39): (10~20): (15~25): (5~25): (1~5): (1 ~8) Mix evenly, then gradually add it dropwise to the reaction kettle, the dropping time is 3~5h;
[0041] (3) After the dropwise addition, keep the temperature at 120~130°C for 1~2h, and lower the temperature in the reactor to 100~120°C;
[0042] (4) Add dimethylethanolamine, stir and neutralize, then add water to disperse the reactants, then cool down to lower the temperature of the materials in the reactor to 30~40°C;
[0043] (5) Filter to obtain the resin dispersion liquid for water-based two-component metal paint. ...
Embodiment 1
[0045] Embodiment 1: the water-based two-component metallic paint resin dispersion liquid of the present embodiment comprises each component of following parts by volume:
[0046] Methyl methacrylate 20 parts
[0047] Styrene 10 parts
[0048] 15 parts of isooctyl acrylate
[0049] 5 parts of hydroxyethyl methacrylate
[0050] 1 part acrylic
[0051] Initiator 1 part
[0052] 1 part solvent
[0053] 1 part solvent gasoline
[0054] The initiator is one or a combination of tert-hexyl peroxytrimethyl acetate, tert-butyl peroxy octanoate and tert-butyl peroxybenzoate.
[0055] The solvent is one or a combination of propylene glycol n-propyl ether, propylene glycol isopropyl ether, propylene glycol n-butyl ether and dipropylene glycol butyl ether.
[0056] The solvent gasoline has a distillation range of 120°C to 200°C.
[0057] The preparation method of above-mentioned water-based two-component metal paint resin dispersion liquid, comprises the steps:
[0058] (1) Add th...
Embodiment 2
[0064]Embodiment 2: the water-based two-component metallic paint resin dispersion of the present embodiment comprises each component of following parts by volume:
[0065] Methyl methacrylate 39 parts
[0066] Styrene 20 parts
[0067] 25 parts of isooctyl acrylate
[0068] 25 parts of hydroxyethyl methacrylate
[0069] Acrylic 5 parts
[0070] Initiator 8 parts
[0071] Solvent 15 parts
[0072] Solvent gasoline 20 parts
[0073] Wherein, the initiator is one or a combination of tert-hexyl peroxytrimethyl acetate, tert-butyl peroxy octanoate, and tert-butyl peroxybenzoate.
[0074] Wherein, the solvent is one or a combination of propylene glycol n-propyl ether, propylene glycol isopropyl ether, propylene glycol n-butyl ether, and dipropylene glycol butyl ether.
[0075] Wherein, the solvent gasoline has a distillation range of 120°C to 200°C.
[0076] The preparation method of above-mentioned water-based two-component metal paint resin dispersion liquid, comprises the...
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