A lithium-sulfur battery cathode copolymerized sulfur material and a lithium-sulfur battery made of it
A lithium-sulfur battery and positive electrode technology, applied in the field of energy materials, to achieve the effects of easy operation, large-scale production, and cheap and easy-to-obtain raw materials
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Embodiment 1
[0040] (1) Add 0.5g valeronitrile to 4.5g sublimated sulfur powder, and carry out low-speed ball milling to it for 4h, (the ball milling speed is 400r / min, every ten minutes interval of ball milling is 3 minutes) to obtain a stable homogeneous mixture;
[0041] (2) Heat the mixture obtained in step (1) to 120° C. at a heating rate of 10° C. / min.
[0042] (3) The mixture obtained in step (2) was kept at 120° C. and stirred for 6 h.
[0043] (4) The mixture obtained in step (3) was cooled to room temperature and then ball milled for 4 hours (the ball milling speed was 400 r / min, and the milling interval was 3 minutes every 10 minutes).
[0044] For pictures of sublimated sulfur powder see figure 1 The leftmost sample, the second from the left is the photo of the copolymerized sulfur product in which valeronitrile made in this embodiment accounts for 10%. figure 2 It is an electron micrograph of the copolymerized sulfur product, and it can be seen that the particle size of the...
Embodiment 2
[0049] (1) Add 1g of valeronitrile to 4g of sublimated sulfur powder, and carry out low-speed ball milling to it for 4h to obtain a stable homogeneous mixture;
[0050] (2) Heat the mixture obtained in step (1) to 120° C. at a heating rate of 10° C. / min.
[0051] (3) The mixture obtained in step (2) was kept at 120° C. and stirred for 6 h.
[0052] (4) The mixture obtained in step (3) was cooled to room temperature and ball milled for 4 hours.
[0053] figure 1 The third sample from the left is a photo of the copolymerized sulfur product in which valeronitrile produced in this example accounts for 20%. image 3 It is an electron micrograph of the copolymerized sulfur product. It can be seen from the figure that the copolymerized sulfur is in an agglomerated state, with a large particle size and a small amount of granular protrusions on the surface. Figure 4 is the XRD pattern of the product. Figure 5 As a result of the thermogravimetric analysis experiment on the product...
Embodiment 3
[0056] (1) Add 1.5g valeronitrile to 3.5g sublimated sulfur powder, and carry out low-speed ball milling to it for 4h at a ball milling speed of 400r / min to obtain a stable homogeneous mixture;
[0057] (2) Heat the mixture obtained in step (1) to 120° C. at a heating rate of 10° C. / min.
[0058] (3) The mixture obtained in step (2) was kept at 120° C. and stirred for 6 h.
[0059] (4) The mixture obtained in step (3) was cooled to room temperature and ball milled for 4 hours.
[0060] figure 1 The rightmost sample is a photo of the copolymerized sulfur product in which valeronitrile produced in this embodiment accounts for 30%. Figure 4 is the XRD pattern of the product. Figure 5 As a result of the thermogravimetric analysis experiment on the product obtained in this example, the polymerized sulfur samples of 10wt.%, 20wt.% and 30wt.% valeronitrile at 0-650°C began to lose weight at about 130°C, which basically guaranteed the battery preparation process. thermal stabili...
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