Electret nanofiber filter material for automobile air conditioning filter elements and preparation method thereof
A technology of nanofibers and automotive air conditioners, which is applied in the fields of filtration and separation, membrane filters, separation methods, etc., and can solve the problems of limiting the effect of automotive air conditioning filters on air quality improvement, easy failure service life, and huge impact
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Embodiment 1
[0053] A method for preparing an electret nanofiber filter material for an automotive air-conditioning filter, the specific steps of which are as follows:
[0054] (1) Prepare a liquid mixture in which the polymer is dissolved: add polyvinylidene fluoride to N,N-dimethylformamide, and continuously stir for 11 hours with a magnetic stirring device;
[0055] (2) Electrospinning is carried out after heating the polymer-dissolved liquid mixture with a mass concentration of 22% to 50°C, and the polymer-dissolved liquid mixture in the spinneret hole is rapidly solidified during the electrospinning process, wherein Rapid solidification means that the temperature of the liquid mixture dissolved in the polymer is raised to 80°C within 0.1ms at the outlet of the spinneret 3cm, and to 125°C within 0.9ms at the outlet of 10cm of the spinneret. The process parameters of electrospinning are : The voltage is 50KV, the receiving distance is 20cm, the perfusion rate is 0.1mL / h, the temperature...
Embodiment 2~24
[0061] A kind of preparation method of electret nanofiber filter material for automobile air conditioner filter element, its specific steps are consistent with embodiment 1, difference is the kind of polymer and solvent selected when step (1) prepares the liquid mixture that dissolves polymer , the temperature of the stage heating and the performance of the final product, see the table below for details. In the table, T1 (°C) represents the temperature of the first stage of heating, T2 (°C) represents the temperature of the second stage of heating, and A represents the surface static electricity Potential, B represents the filtration efficiency of particles from 0.006 to 1 μm, the unit of fiber diameter is μm, and the unit of pore size is μm; the unit of nanofiber diameter of nanofiber layer is μm, and the unit of nanofiber gram weight is g / m 2 , the unit of porosity is %; the unit of A is V, the unit of hydrophobic angle is (°), the unit of B is %, the unit of piezoresistance ...
Embodiment 25
[0065] A method for preparing an electret nanofiber filter material for an automotive air-conditioning filter, the specific steps of which are as follows:
[0066] (1) Prepare a liquid mixture in which the polymer is dissolved: add polyvinylidene fluoride to N-methylpyrrolidone, and continuously stir for 18 hours with a magnetic stirring device;
[0067] (2) Electrospinning is carried out after heating the polymer-dissolved liquid mixture with a mass concentration of 36% to 85°C, and the polymer-dissolved liquid mixture in the spinneret hole is rapidly solidified during the electrospinning process, wherein Rapid solidification means that the temperature of the liquid mixture dissolved in the polymer is raised to 105°C within 0.9ms at the outlet of the spinneret hole 5cm, and to 155°C within 0.1ms at the outlet of the spinneret hole 9cm. The process parameters of electrospinning are : The voltage is 20KV, the receiving distance is 10cm, the perfusion rate is 5.2mL / h, the temper...
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