Preparation method of thermoplastic carbon fiber composite material for medical instruments
A technology of medical devices and composite materials, which is applied in the field of preparation of carbon fiber composite materials for thermoplastic medical devices, can solve problems such as difficult secondary shaping, achieve good compatibility, good promotion and use value, and reduce pain.
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Embodiment 1
[0025] 1) Preparation of prepreg by melting impregnation: melt the sheet-like thermoplastic PEK resin matrix (content 60%) at a temperature of 400°C, and then impregnate acrylonitrile-based carbon fibers through the molten resin at a speed of 5cm / s, The resin-impregnated fiber is cooled to obtain a prepreg;
[0026] 2) Laying: Take the medical device model prosthesis, and lay carbon fiber prepreg on the inner layer of the prosthesis mold, 15 layers of prepreg for the leg prosthesis, and 12 layers of prepreg for the hand;
[0027] 3) Molding: Molding is carried out by melting and pressing. The heat source of the melting and pressing is electric conduction heating. The prosthetic mold is energized, and the temperature of the melting and pressing is set to 300°C, the pressure is 35 MPa, and the time is 45 minutes.
Embodiment 2
[0029] 1) Preparation of prepreg by fluidized bed impregnation: pass each bundle of acrylonitrile-based carbon fiber through a fluidized bed with thermoplastic PEK resin powder (content 60%), and the resin powder is suspended in one or more air streams, and the air stream is in Pass through the fiber under controlled pressure, and the resin powder deposited on the carbon fiber will be deposited on the carbon fiber, then heated to a temperature of 400°C in a melting furnace to melt the resin and adhere to the carbon fiber, and then pass through the cooling and shaping section to make the surface uniform and smooth , and finally wind up the prepreg through the winding device;
[0030] 2) Laying: Take the medical device model, such as prosthesis, bone plate, etc., lay carbon fiber prepreg on the inner layer of the prosthesis mold and the surface of the bone plate, use 15 layers of prepreg for the leg prosthesis, and use 12 layers of prepreg for the hand. layer;
[0031] 3) Moldi...
Embodiment 3
[0033] 1) Preparation of prepreg by melting impregnation: melt the plate-like thermoplastic PP resin matrix (content 50%) at a temperature of 500°C, and then add acrylonitrile-based carbon fibers, pitch-based carbon fibers and viscose-based carbon fibers at 5cm / The speed of s is impregnated by molten resin, and the resin-impregnated fiber is cooled to obtain a prepreg;
[0034] 2) Laying: Take the medical device model prosthesis, and lay carbon fiber prepreg on the inner layer of the prosthesis mold, 15 layers of prepreg for the leg prosthesis, and 12 layers of prepreg for the hand;
[0035] 3) Molding: Molding is performed by melting and pressing. The heat source of the melting and pressing is electric conduction heating. The prosthesis mold is energized, and the temperature range of the melting and pressing is set to 400°C, the pressure range is 10 MPa, and the time is 45 minutes.
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