Pixel defining layer, preparation method thereof and display device
A pixel definition layer and display device technology, which is applied in semiconductor/solid-state device manufacturing, electrical components, electric solid-state devices, etc., can solve problems such as the difficulty of printing uniform thin films, achieve the effect of improving uniformity and solving the problem of printing uniform thin films
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Embodiment 1
[0049] Dissolve epoxy resin EPON826 in methyl isobutyl ketone solvent, put it in a three-necked flask, stir and heat to 70~80°C, according to the mass ratio of epoxy resin to sodium azide 1:1, add sodium azide Soluble in the mixture of water and methyl isobutyl ketone, and slowly add dropwise to the three-necked flask, the dropping time is 0.5~2h, continue to react for 1~3h after the dropwise addition, and then distill under reduced pressure to remove methyl isobutyl base ketone and water, and dissolve the solid in methyl isobutyl ketone, filter to remove sodium azide, obtain azide epoxy resin after vacuum distillation again;
[0050] Heat the azide epoxy resin to 70~80°C to melt, then mix the azide epoxy resin, polyoxypropylene diamine epoxy curing agent, and decylamine in a molar ratio of 4:1:2, and then inject placed in a mold on the substrate, cured for 1 to 2 hours at 100 to 110 degrees Celsius, and then cured for 1 to 2 hours at 130 to 140 degrees Celsius, and an initial...
Embodiment 2
[0053] Dissolve epoxy resin E-51 in methyl isobutyl ketone solvent, put it in a three-necked flask, stir and heat to 60~70°C, according to the mass ratio of epoxy resin to sodium azide 1:1, add azide Dissolve sodium chloride in a mixture of water and methyl isobutyl ketone, and slowly add it dropwise to a three-necked flask for 0.5~2 hours. After the dropwise addition, continue to react for 1~3 hours, and then distill under reduced pressure to remove methyl Isobutyl ketone and water, and dissolve solid in methyl isobutyl ketone, filter to remove sodium azide, obtain azide epoxy resin after vacuum distillation again;
[0054] Heat the azide epoxy resin to 70~80°C to melt, then mix the azide epoxy resin, polyoxypropylene diamine epoxy curing agent, and decylamine in a molar ratio of 4:1:2, and then inject placed in a mold on the substrate, cured for 1 to 2 hours at 100 to 110 degrees Celsius, and then cured for 1 to 2 hours at 130 to 140 degrees Celsius, and an initial pixel def...
Embodiment 3
[0057] Dissolve epoxy resin EPON826 in methyl isobutyl ketone solvent, put it in a three-necked flask, stir and heat to 70~80°C, according to the mass ratio of epoxy resin to sodium azide 1:1, add sodium azide Soluble in the mixture of water and methyl isobutyl ketone, and slowly add dropwise to the three-necked flask, the dropping time is 0.5~2h, continue to react for 1~3h after the dropwise addition, and then distill under reduced pressure to remove methyl isobutyl base ketone and water, and dissolve the solid in methyl isobutyl ketone, filter to remove sodium azide, obtain azide epoxy resin after vacuum distillation again;
[0058] Heat the azide epoxy resin to 70~80°C to melt, and then mix the azide epoxy resin, methyltetrahydrophthalic anhydride, 2-ethyl-4- Methylimidazole is mixed evenly and placed in an oven at 80 degrees Celsius to stand still. After the air bubbles are removed, it is then injected into a mold placed on the substrate, cured at 80~90 degrees Celsius for...
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