A kind of Hericium erinaceus polysaccharide chelated zinc microcapsule and preparation method thereof
A technology of Hericium erinaceus polysaccharide and chelated zinc, applied in microcapsules, capsule delivery, drug combination and other directions, can solve the problems of prolonged shelf life, low zinc content, poor antioxidant activity, etc. Antioxidative effect enhancement, the effect of wide practical value
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Embodiment 1
[0045] Example 1: Preparation of Hericium erinaceus polysaccharide chelated zinc microcapsules
[0046] The invention provides a preparation method of Hericium erinaceus polysaccharide chelated zinc microcapsules, which specifically adopts the following technical steps:
[0047] (1) Preparation of Hericium erinaceus polysaccharide chelated zinc (Zn-HEP): configuration concentration is 12.5g / L-17.5g / L Hericium erinaceus polysaccharide solution, gets 20mL-30mL polysaccharide solution, adds 20mL-30mL concentration to be 0.4mol / L-0.5mol / L ZnSO 4 Solution, stirred and reacted at 30°C-50°C for 2h-4h, the reaction solution was dialyzed through running water for 7h-9h, and dried to obtain Hericium erinaceus polysaccharide chelated zinc (Zn-HEP), the zinc content was 4mg / g-6mg / g.
[0048] (2) Preparation of Hericium erinaceus polysaccharide chelated zinc microcapsules: Carrageenan, chitosan and β-cyclodextrin are used as wall materials, the core-to-wall ratio is 1:9-1:11, and the so...
Embodiment 2
[0056] Embodiment two: the preparation of Hericium erinaceus polysaccharide (HEP)
[0057] The purchased Hericium erinaceus is dried, crushed, and passed through a 60-mesh sieve to obtain dried Hericium erinaceus powder. Extract Hericium erinaceus powder and distilled water in hot water at 90°C for 3 hours at a solid-liquid ratio of 1:30. The extract was centrifuged at 4000r / min for 10min, the precipitate was discarded and the supernatant was combined. The combined supernatant was rotary evaporated to 1 / 3 of the original volume, and 4 times the volume of 95% ethanol was added to precipitate overnight, and the precipitate was collected after centrifugation. After drying, it was Hericium erinaceus crude polysaccharide (HEP).
[0058] Reconstitute the dried HEP with distilled water to remove protein, add Sevage reagent (n-butanol: chloroform = 1:4) to 1 / 4 volume of the concentrated liquid, stir at room temperature for 20 min, centrifuge at 2600 r / min, and combine supernatant. ...
Embodiment 3
[0060] Embodiment three: the preparation of Hericium erinaceus polysaccharide chelated zinc (Zn-HEP)
[0061] Configure the Hericium erinaceus polysaccharide solution with a concentration of 7.5g / L, take 35mL of the polysaccharide solution, add 30mL of ZnSO with a concentration of 0.35mol / L 4 The solution was stirred and reacted at 30°C for 6h. The reaction solution was dialyzed under running water for 6 hours, and then dried to obtain the chelated zinc of Hericium erinaceus polysaccharide (Zn-HEP).
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