Low refractive index film and centrifuge container for producing the same
A low-refractive-index film and centrifugal container technology, which is applied in the field of centrifugal containers, can solve problems such as unsatisfactory low-refractive-index films, insufficient adhesion of low-refractive-index films, and low-refractive-index requirements.
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Embodiment 1
[0053] A low refractive index film, the main raw materials include: 15 parts of silica sol, 20 parts of polytetrafluoroethylene suspension (concentrated), 10 parts of diluent, appropriate amount of pH regulator; also includes polytetrafluoroethylene film as the bottom film ; pH regulator is preferably volatile substances, such as ammonia and the like.
[0054] The silica sol contains spherical colloidal silica particles and elongated amorphous colloidal silica particles, wherein the content ratio of spherical colloidal silica particles and elongated amorphous colloidal silica particles is 1:1;
[0055] The average particle diameter D1 of the spherical colloidal silica particles measured by the dynamic light scattering method is 50-100 nm;
[0056] The ratio of the particle diameter D2 measured by the dynamic light scattering method of the elongated amorphous colloidal silica particles to the particle diameter D3 measured by the nitrogen adsorption method is greater than 5, and...
Embodiment 2
[0070] When the film B is used as a low-refractive-index adhesive layer between two objects, the film B is pasted on the surface of an object, the temperature is raised to above 327°C, another object is buckled on the film B, and after a period of heat preservation, it is quickly cool down.
[0071] Due to the high adhesion on both sides of the low-refractive index film, it can be used as a low-refractive index bonding layer. It can replace OCA optical glue. When sintering to form a film, stick the film B on the glass cover, raise the temperature to 340°C, buckle the substrate on the film B (attached to the glass cover), keep warm and hot press for 60s under vacuum conditions, and then cool rapidly; such as the substrate If it is difficult to withstand high temperature, after the temperature rises to above 327°C, it can be kept under vacuum for tens of seconds, and then quickly cooled to about 200°C, and the substrate and glass cover are bonded together, heat-preserved, hot-p...
Embodiment 3
[0073] Such as Figure 1-3 Shown, a kind of centrifuge container used for preparing film B comprises centrifuge container body 1 and cover 2, and described centrifuge container body is the arc-shaped plate-shaped container that tool inner chamber 5, curvature and the centrifuge tank adapt, centrifuge One side of the outer wall of the container is provided with upward liquid inlet and outlet nozzles 3 and air inlet and outlet nozzles 4, the inlet and outlet air nozzles are connected to the inner cavity, and the liquid inlet and outlet nozzles are connected to the inner cavity through the extension tube 6 arranged on the inner wall of the centrifuge container; The liquid inlet and outlet nozzles facilitate the liquid inlet and pumping operations, and the air inlet and outlet nozzles are used to balance the internal and external air pressure. The arc-shaped design makes the centrifuge container close to the inner wall of the container tank during centrifugation, reducing and avoi...
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