A Copper(i) Alkyne Cluster with Aggregation-Induced Luminescence and Circularly Polarized Luminescence
A technology of nano-copper clusters and copper atoms, applied in the field of copper alkyne clusters, to achieve good application value, high chiral luminescence characteristics, and good biocompatibility
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Embodiment 1
[0023] Embodiment 1: the synthesis of nano-copper cluster material of the present invention
[0024] Dissolve 0.035 mmol of (R / S)-2-diphenyl-hydroxymethylpyrrolidine-1-propyne (R / S-DPM) and 0.035 mmol of tetraacetonitrile copper hexafluorophosphate in a mixture of 2 mL of toluene and 2 mL of acetone In the solution, stir the solution quickly to clarify. After the reaction, place the clear solution at room temperature to avoid light and volatilize. After 2 days, orange blocky crystals are obtained. The yield is 50%. Filter, wash with ethanol, and dry at room temperature for its property test Material.
[0025] Get the nano copper cluster material of the present invention that embodiment 1 makes and do further characterization, its process is as follows:
[0026] (1) Determination of crystal structure
[0027] The X-ray single crystal diffraction data of the complexes were measured on a Rigaku XtaLAB Pro single crystal diffractometer with a single crystal sample of appropriate...
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