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Preparation method and application of celery seed oil resin for cigarette

A technology of celery seed oil and celery seed, which is applied in the fields of application, tobacco, and tobacco treatment, can solve the problems of irritation, monotonous aroma, and single effect of smoke, so as to avoid pollution, soft smoke, and reduce suction stimulation Effect

Active Publication Date: 2019-11-26
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These two types of flavors are used alone or blended, although the process is simple, but the aroma is monotonous, stimulating, and has a single effect on smoke.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A preparation method of celery seed oleoresin for cigarettes, the steps are as follows:

[0028] (1) Wash and remove impurities from celery seeds.

[0029] (2) Put clean celery seeds into a pressure vessel, set the puffing pressure to 3Mpa, puffing temperature to 35°C, and puffing treatment for 10 min.

[0030] (3) Then crush the puffed celery seeds to 60 mesh.

[0031] (4) Put the obtained celery seed powder in an ultrasonic device, add ethanol solvent, and the ratio of solid to liquid is 1:6. Set the ultrasonic power to 200W, and conduct ultrasonic extraction for 40 minutes at a temperature of 40°C.

[0032] (5) Centrifuge the ultrasonicated material, set the centrifugal speed to 800r / min, the centrifugal power to 150W, and the centrifugal time to 10min, and collect the filtrate.

[0033] (6) After the filtrate obtained by using the Buchner funnel is filtered again, the obtained secondary filtrate is placed in a low-temperature vacuum and concentrated to 1 / 8 of the...

Embodiment 2

[0036] A preparation method of celery seed oleoresin for cigarettes, the steps are as follows:

[0037] (1) Wash and remove impurities from celery seeds.

[0038] (2) Put clean celery seeds into a pressure vessel, set the puffing pressure to 10Mpa, puffing temperature to 40°C, and puffing treatment for 15 minutes.

[0039] (3) Then crush the puffed celery seeds to 100 mesh.

[0040] (4) Put the obtained celery seed powder in an ultrasonic device, add ethanol solvent, and the ratio of solid to liquid is 1:10. Set the ultrasonic power to 250W, and conduct ultrasonic extraction for 50 minutes at a temperature of 50°C.

[0041] (5) Centrifuge the ultrasonicated material, set the centrifugal speed to 1000r / min, the centrifugal power to 200W, and the centrifugal time to 15min, and collect the filtrate.

[0042] (6) After the filtrate obtained by using the Buchner funnel is filtered again, the obtained secondary filtrate is placed in a low-temperature vacuum and concentrated to 1 / ...

Embodiment 3

[0045] A preparation method of celery seed oleoresin for cigarettes, the steps are as follows:

[0046] (1) Wash and remove impurities from celery seeds.

[0047] (2) Put clean celery seeds into a pressure vessel, set the puffing pressure to 8Mpa, puffing temperature to 38°C, and puffing treatment for 12 minutes.

[0048] (3) Then crush the puffed celery seeds to 80 mesh.

[0049] (4) Put the obtained celery seed powder in an ultrasonic device, add ethanol solvent, and the ratio of solid to liquid is 1:8. Set the ultrasonic power to 230W, and conduct ultrasonic extraction for 45 minutes at a temperature of 45°C.

[0050] (5) Centrifuge the ultrasonicated material, set the centrifugal speed to 900r / min, the centrifugal power to 170W, and the centrifugal time to 13min, and collect the filtrate.

[0051] (6) After the filtrate obtained by using the Buchner funnel is filtered again, the obtained secondary filtrate is placed in a low-temperature vacuum and concentrated to 1 / 7 of...

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PUM

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Abstract

The invention relates to the technical field of cigarette flavor, in particular to a preparation method and application of celery seed oil resin for cigarette. The preparation method of the celery seed oil resin comprises the following steps of (1) carrying out cleaning and impurity removing on celery seeds; (2) carrying out high-pressure puffing treatment on the celery seeds, and then crushing; and (3) mixing the obtained celery seed powder with ethyl alcohol, and carrying out extraction for 40-50min at a temperature of 40-45 DEG C, and next, performing centrifuging, and collecting the filtrate. According to the method, the pure physical extraction method is adopted, the crushing of the celery seeds is realized through the puffing treatment, and an ultrasonic extraction method can extendinto the cells of the materials, so that the extraction rate of the effective components is greatly improved, the nutrition and fragrance of the celery seeds are kept, and the pollution is reduced. Meanwhile, the celery seed oil resin prepared by the method disclosed by the invention is used in cut tobacco, so that the cigarette smoke can be softer, and the suction irritation is reduced.

Description

technical field [0001] The invention relates to the technical field of tobacco spices, in particular to a preparation method and application of celery seed oleoresin for tobacco. Background technique [0002] At present, the tobacco flavors used in cigarettes in my country generally adopt two categories: one is natural extraction flavors, which use natural components contained in natural flavors or potentially coordinated with smoke; the other is synthetic flavors, which use synthetic It is a fragrance monomer that coordinates with the smoke and has a certain effect on the smoke. The flavors for tobacco produced by these two types of spices alone or by blending are simple in process, but have the problems of monotonous and irritating aroma and single effect on smoke. The research on tobacco spices in our country has always been relatively backward, and most of the spices depend on imports. Therefore, it is necessary to develop tobacco flavors that can make smoke soft and del...

Claims

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Application Information

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IPC IPC(8): A24B15/20A24B15/18A24B15/30
CPCA24B15/18A24B15/20A24B15/303A24B15/305
Inventor 苗丽坤蹇顺华刘娇等程书锋陈胜
Owner HUBEI CHINA TOBACCO IND
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