A kind of hybrid porous monolithic material and its preparation and application
A monolithic material and hybridization technology, applied in chemical instruments and methods, and other chemical processes, can solve the problems of poor mechanical strength, easy swelling, and poor stability of organic monolithic columns, and achieve shortened preparation time and thermal stability Good performance and strong versatility
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[0024] Preparation of POSS-SH functional monomer: First, take 15mL of mercaptopropyltrimethoxysilane (MPTS) and dissolve it in 360mL of methanol, add 30mL of concentrated hydrochloric acid (36% to 38%) dropwise to the solution, and in an oil bath at 90°C Reflux reaction for 24h; after the reaction is completed, cool the reaction solution in an ice bath (-4°C-4°C) to obtain a crude product, wash the crude product three times with methanol to remove residual mercaptopropyltrimethoxysilane; then, use di Dissolve the obtained crude product in methyl chloride, add water to the solution for extraction, collect the dichloromethane layer, then add water for extraction, repeat three times, finally collect dichloromethane, add anhydrous sodium sulfate to it and dry overnight; finally, the obtained The solution was distilled under reduced pressure to obtain the product POSS-SH. The obtained POSS-SH was dissolved in tetrahydrofuran solution (50.0%, w / v, mg / ml) for use.
[0025] The prepa...
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