A kind of preparation method of lipophilic hyperbranched molecular modification nanofluid
A nanofluid and lipophilic technology, applied in the field of heat transfer, can solve the problems of difficult to guarantee the stability of nanofluid and the influence of nanofluid heat transfer ability, etc., and achieve the effect of easy popularization and application, prolonging life, and simple steps
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Embodiment 1
[0034] The preparation method of the lipophilic hyperbranched molecular modified nanofluid of the present embodiment is as follows:
[0035] (1) Add 10 g of hexadecyl chloride to 40 mL of chloroform, under nitrogen protection, dissolve 2 g of PEI (number average molecular weight distribution 1000-36000) in chloroform and add to the above solution, then add 5 g of triethyl amine, the mixture was vigorously stirred at 0°C for 3 h, then the mixture was reacted at 25°C for 24 h, and finally reacted at 70°C for 2 h to obtain a crude product; then, the crude product was cooled to room temperature, and the waste residue was removed by suction filtration. Stir for 1 h, discard the upper layer of acetone, repeat the washing twice, 35 ° C rotary evaporation and vacuum drying to obtain HPEI-C16;
[0036] (2) Add 0.4 g tetra-n-octylammonium bromide and 0.2 g potassium chloropalladate to 120 mL toluene, and react for 1 h. Take the organic phase, add 0.2 g HPEI-C16, add 20 mL NaBH dropwise...
Embodiment 2
[0040] The preparation method of the lipophilic hyperbranched molecular modified nanofluid of the present embodiment is as follows:
[0041] (1) Add 0.3 g tetra-n-octylammonium bromide and 0.1 g potassium chloropalladate to 120 mL toluene, and react for 1 h. Take the organic phase, add 0.2 g of HPEI-C16 obtained in Example 1, add 20 mL of NaBH dropwise 4 Aqueous solution (0.1 g / 10 mL water), stirring vigorously for 12 h, standing still to take the organic layer; rotary evaporation at 45 ℃ to get the crude product, washing with absolute ethanol 3 times, drying in vacuum overnight at 25 ℃ to obtain lipophilic hyperbranched molecular modification nanoparticles;
[0042] (2) The nanoparticles obtained in step (1) were weighed, added to decahydronaphthalene for ultrasonic dispersion for 1 h, and a lipophilic hyperbranched molecule-modified nanofluid with a nanoparticle content of 0.01% to 0.5% was obtained.
[0043] The palladium nanofluid can exist stably for more than one month...
Embodiment 3
[0045] The preparation method of the lipophilic hyperbranched molecular modified nanofluid of the present embodiment is as follows:
[0046] (1) Add 0.3 g tetra-n-octylammonium bromide and 0.4 g potassium chloropalladate to 120 mL toluene, and react for 1 h. Take the organic phase, add 0.2 g of HPEI-C16 obtained in Example 1, add 20 mL of NaBH dropwise 4 Aqueous solution (0.1 g / 10mL water), stirring vigorously for 12 h, standing still to take the organic layer; 45 ℃ rotary evaporation to get the crude product, washing with absolute ethanol 3 times, vacuum drying at 25 ℃ overnight to obtain lipophilic hyperbranched molecular modified nano particles.
[0047] (2) The nanoparticles obtained in step (1) were weighed, added to decahydronaphthalene for ultrasonic dispersion for 1 h, and a lipophilic hyperbranched molecule-modified nanofluid with a nanoparticle content of 0.01% to 0.3% was obtained.
[0048] The palladium nanofluid can exist stably for more than 15 days, and the th...
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