Preparation method of algistat containing gingko endophyte
A technology of endophytic bacteria and anti-algae agent, which is applied in the field of preparation of endophytic anti-algae agent containing ginkgo biloba, which can solve the problems of slow effect of algae inhibitor and short time for algae removal
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[0030] Example 1
[0031] Preparation of heat treatment reaction solution:
[0032] Put ginkgo bark and ginkgo leaves into a pulverizer at a mass ratio of 5:1 to pulverize to obtain a mixture, put the mixture into an oven, and dry it for 2 hours at a temperature of 40 °C to obtain a dry material. Anhydrous ethanol was put into a beaker at a mass ratio of 1:10, the beaker was placed in a shaker, shaken and soaked for 3 hours, and after soaking, the filter residue and filtrate were obtained by suction filtration and separated for use;
[0033] The above filter residue was put into the reaction kettle, soaked with hydrochloric acid with a mass fraction of 3%, the reaction kettle was sealed, the temperature in the reaction kettle was raised to 60 ° C, and the stirring speed was 400 r / min under constant temperature conditions for 2 hours. Add 10% sodium hydroxide solution dropwise to the beaker to adjust the pH to 10 to obtain an alkaline mixed solution;
[0034] The above-mentio...
Example Embodiment
[0040] Example 2
[0041] Preparation of heat treatment reaction solution:
[0042] Put ginkgo bark and ginkgo leaves into a pulverizer at a mass ratio of 5:1 to pulverize to obtain a mixture, put the mixture into an oven, and dry it at a temperature of 45 ° C for 2.5 hours to obtain a dry material. Put it into a beaker with anhydrous ethanol in a mass ratio of 1:10, place the beaker in a shaker, shake and soak for 3.5 hours, and then separate by suction filtration to obtain filter residue and filtrate, which are for later use;
[0043] The above filter residue was put into the reaction kettle, soaked in hydrochloric acid with a mass fraction of 5%, the reaction kettle was sealed, the temperature in the reaction kettle was raised to 65 ° C, and the stirring speed was 450 r / min under constant temperature conditions for 2.5 h, stirring. Then, add 12% sodium hydroxide solution dropwise to the beaker to adjust the pH value to 11 to obtain an alkaline mixed solution;
[0044] The...
Example Embodiment
[0050] Example 3
[0051] Preparation of heat treatment reaction solution:
[0052] Put ginkgo bark and ginkgo leaves into a pulverizer in a mass ratio of 5:1 to pulverize to obtain a mixture, put the mixture into an oven, and dry it for 3 hours at a temperature of 50 ° C to obtain a dry material. Anhydrous ethanol was put into a beaker at a mass ratio of 1:10, the beaker was placed in a shaker, and soaked for 4 hours in a shaker. After soaking, suction filtration was performed to separate the filter residue and filtrate, which were used for later use;
[0053] The above filter residue was put into the reaction kettle, soaked in hydrochloric acid with a mass fraction of 6%, the reaction kettle was sealed, the temperature in the reaction kettle was raised to 70 ° C, and the stirring speed was 500 r / min under constant temperature conditions for 3 hours. Add 15% sodium hydroxide solution dropwise to the beaker to adjust the pH to 12 to obtain an alkaline mixed solution;
[0054...
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