Preparation method of algistat containing gingko endophyte
A technology of endophytic bacteria and anti-algae agent, which is applied in the field of preparation of endophytic anti-algae agent containing ginkgo biloba, which can solve the problems of slow effect of algae inhibitor and short time for algae removal
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Embodiment 1
[0031] Preparation of heat treatment reaction solution:
[0032] Ginkgo bark and ginkgo leaves are put into pulverizer according to the mass ratio of 5:1 to make a mixture, put the mixture into an oven, and dry for 2 hours at a temperature of 40°C to obtain a dry material, and mix the dry material with Put absolute ethanol into a beaker at a mass ratio of 1:10, place the beaker in a shaker, oscillate and soak for 3 hours, and after soaking, filter with suction to separate the filter residue and filtrate, and set aside;
[0033] Put the above filter residue into the reaction kettle, soak it with hydrochloric acid with a mass fraction of 3%, seal the reaction kettle, raise the temperature inside the reaction kettle to 60°C, and stir with a stirrer at a speed of 400r / min for 2 hours under constant temperature conditions. After stirring, Dropwise add a mass fraction of 10% sodium hydroxide solution to the beaker to adjust the pH value to 10 to prepare an alkaline mixed solution; ...
Embodiment 2
[0041] Preparation of heat treatment reaction solution:
[0042] Ginkgo bark and ginkgo leaves are put into the pulverizer according to the mass ratio of 5:1 and pulverized to obtain a mixture, the mixture is put into an oven, and dried for 2.5 hours at a temperature of 45°C to obtain a dry material, and the dried material Put it into a beaker with anhydrous ethanol at a mass ratio of 1:10, place the beaker in a shaker, oscillate and soak for 3.5 hours, after soaking, filter and separate by suction to obtain the filter residue and filtrate, and set aside;
[0043] Put the above filter residue into the reaction kettle, soak it with hydrochloric acid with a mass fraction of 5%, seal the reaction kettle, raise the temperature in the reaction kettle to 65°C, stir with a stirrer at a speed of 450r / min for 2.5h under constant temperature conditions, and stir Afterwards, dropwise add a mass fraction of 12% sodium hydroxide solution to the beaker to adjust the pH value to 11 to prepar...
Embodiment 3
[0051] Preparation of heat treatment reaction solution:
[0052] Put the ginkgo bark and ginkgo leaves into the pulverizer at a mass ratio of 5:1 to make a mixture, put the mixture into an oven, and dry it for 3 hours at a temperature of 50°C to obtain a dry material, and mix the dry material with Put absolute ethanol into a beaker at a mass ratio of 1:10, place the beaker in a shaker, oscillate and soak for 4 hours, and after soaking, filter with suction to separate the filter residue and filtrate for later use;
[0053] Put the above filter residue into the reaction kettle, soak it with hydrochloric acid with a mass fraction of 6%, seal the reaction kettle, raise the temperature in the reaction kettle to 70°C, and stir with a stirrer at a speed of 500r / min for 3h under constant temperature conditions. After stirring, Dropwise add a mass fraction of 15% sodium hydroxide solution to the beaker to adjust the pH value to 12 to prepare an alkaline mixed solution;
[0054] Put th...
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