Monoclonal antibody against echo30, preparation method and application thereof
A technology of monoclonal antibody and antigen, applied in the field of biomedicine, can solve the problems of non-specific antibody reports, less Echo30 virus, etc.
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Embodiment 1
[0088] Embodiment 1 monoclonal antibody preparation
[0089] 1. Immunogen (antigen): Echo30.
[0090] Each mouse was immunized 5 times, each time with 100 μl of antigen, and a total of 3-3.5ml of virus was needed.
[0091] 2. Animal immunity
[0092] Two adjuvants were used for immunization, namely modified Freund's adjuvant and aqueous adjuvant, two groups were immunized with virus, and each group of 3 mice was used as one adjuvant, and a total of 6 mice were immunized with virus. All immunizations were performed in SPF animal rooms.
[0093] Select 6 Balb / c mice (female mice) aged 5-8 weeks, mix the immunogen and adjuvant and then emulsify them separately for immunization. Freund's complete adjuvant is used for the first injection, and Freund's complete adjuvant is used for the next 4 booster injections. Incomplete adjuvant, mixed well with the same volume of antigen before injection.
[0094] The immunization method is multi-point injection on the back, the main injecti...
Embodiment 2
[0121] Example 2 Antibody function
[0122] 1. Antigen-antibody affinity determination
[0123] 1.1 Surface plasmon resonance (SPR)
[0124] 1.1.1 Steps:
[0125] Cut and purify 4B10-IgG (full-length antibody) and 6C5-IgG (full-length antibody) using Pierce Fab Preparation Kit (Thermo) to obtain 4B10-Fab (Fab fragment of antibody) and 6C5-Fab (Fab fragment of antibody) .
[0126] SPR experiments were performed using BIAcore T100 (Biacore, GE Healthcare), and the buffer was PBS containing 0.05% Tween-20. Purified E30 whole virus particles were immobilized on the surface of a CM5 sensor chip using the NHS / EDC method until the RU value reached 740. Gradient concentrations of IgG or Fab were then flowed through the chip at a rate of 20 μl / min, and the chip was regenerated using 10 mM glycine-HCl (pH 1.7) after each injection cycle. Binding affinities were obtained by global fitting of curves using the software BIAevaluation (version 4.1).
[0127] 1.1.2 Results
[0128] The...
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