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Chemical production equipment and using method

A chemical production and equipment technology, applied in the field of chemical production equipment, can solve the problems of volatilization of raw materials and inability to realize continuous production, so as to avoid pollution or loss and improve the efficiency of chemical production

Pending Publication Date: 2020-06-05
ANHUI LIXING CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Generally, for chemical equipment with reaction process and dehydration process at the same time, in order to facilitate the addition of materials such as catalysts in the dehydration process, the reaction process and the dehydration process are generally carried out through two independent equipment, and the dehydration process is carried out manually. In this way, the raw materials produced in the reaction process are added together with catalysts, so continuous production cannot be realized. During the transfer of raw materials between the two devices, it is easy to cause volatilization of raw materials and other situations.

Method used

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  • Chemical production equipment and using method
  • Chemical production equipment and using method
  • Chemical production equipment and using method

Examples

Experimental program
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Effect test

Embodiment 1

[0033] Such as figure 1 as shown, figure 1 It is a structural view of the chemical production equipment; the chemical production equipment of the present invention includes a fixed bed reaction device and a dehydration device, and the fixed bed reaction device and the dehydration device are directly connected through a conduit.

[0034] Specifically, the fixed-bed reactor includes at least two input pipelines 1, a reaction furnace 2, a first condenser 3 and a collector 4, the input pipeline 1 is connected with the inlet of the reaction furnace 2, and the reaction furnace 2 The outlet of the outlet is connected with the collector 4 through the first condenser 3, and the reaction substance is input into the reaction furnace 2 through the input pipe 1 and reacted, liquefied by the condensation effect of the first condenser 3 and Collect in the collector 4, the outlet of the collector 4 is connected with the inlet of the dehydration device.

[0035] The dehydration device includ...

Embodiment 2

[0039] Such as figure 2 as shown, figure 2It is a structural view of the fixed bed reactor; the input pipeline 1 is provided with a filter 12, a switch valve, a pressure reducing valve 13, a flow meter 14, and a one-way valve 15, and the filter 12 is used for filtering the transported There are several on-off valves, among which the first on-off valve 16 is used to control the opening or closing of a single input pipe 1 as a whole, and the second on-off valve 17 and the flow meter 14 are arranged in parallel. The second on-off valve 17 allows the reactant to pass only through the pipeline section provided with the flow meter 14 , so that the flow of the reactant in the input pipeline 1 can be accurately measured. By opening the second on-off valve 17 , to realize the rapid passage of the reactant substance, the one-way valve 15 is used to avoid the reflux of the reactant substance in the input pipeline 1, and the pressure reducing valve 13 is used to adjust the pressure in ...

Embodiment 3

[0046] Such as image 3 as shown, image 3 It is a structural view of the dehydration device; the inlet pipe 10 and the outlet pipe 11 are provided with thermometers near the ends of the membrane module 7 for real-time detection of the temperature of the raw materials entering and leaving from the membrane module 7 .

[0047] The inlet pipe 10 is provided with a pressure gauge for detecting the pressure state of the inlet pipe 10 .

[0048] The inlet pipe 10 is connected to the raw material tank 5 through a return pipe 23, and the return pipe 23 is provided with a return valve 24. When the pressure of the inlet pipe 10 is too high, the return valve 24 is activated to realize the Rapid depressurization of inlet pipe 10. Preferably, the return pipe 23 is also provided with an exhaust valve 25, through which the gas can be quickly discharged due to excessive pressure caused by gasification during the heating process.

[0049] Generally, the connecting ports of the return pipe ...

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Abstract

The invention discloses chemical production equipment and a use method, the chemical production equipment comprises a fixed bed reaction device and a dehydration device, and the fixed bed reaction device is connected with the dehydration device through a conduit; wherein the fixed bed reaction device comprises at least two input pipelines, a reaction furnace, a first condenser and a collector, theinput pipelines are connected with an inlet of the reaction furnace, an outlet of the reaction furnace is connected with the collector through the first condenser, and an outlet of the collector is connected with an inlet of the dehydration device; an outlet of the fixed bed reaction device is connected with a raw material tank, the raw material tank is connected with a membrane assembly throughan inlet pipe and an outlet pipe, the raw material tank and the membrane assembly are arranged in a heating cavity, the membrane assembly is of a cylindrical structure internally provided with a pervaporation membrane, and the membrane assembly is connected with a vacuum assembly and a second condenser; according to the invention, the pervaporation membrane is adopted to carry out the dehydrationprocess, so that the continuous operation from the reaction process to the dehydration process can be realized, the chemical production efficiency is greatly improved, and meanwhile, the pollution orloss in the raw material transfer process is avoided.

Description

technical field [0001] The invention relates to the technical field of chemical production, in particular to a chemical production equipment and a use method. Background technique [0002] Fixed bed reactor, also known as packed bed reactor, is a reactor filled with solid catalyst or solid reactant to realize heterogeneous reaction process. The solids are usually granular, with a particle size of about 2 to 15 mm, and are piled up into a bed of a certain height (or thickness). The bed is stationary and the fluid passes through the bed to react. The difference between it and the fluidized bed reactor and moving bed reactor is that the solid particles are in a static state. Fixed bed reactors are mainly used to realize gas-solid phase catalytic reactions, such as ammonia synthesis towers, sulfur dioxide contact oxidizers, hydrocarbon steam reformers, etc. When used in gas-solid or liquid-solid non-catalytic reactions, the bed is filled with solid reactants. The trickle bed...

Claims

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Application Information

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IPC IPC(8): B01J8/02F26B5/04F26B23/00
CPCB01J8/02F26B5/04F26B23/00
Inventor 汪德林邵千飞黄绪民
Owner ANHUI LIXING CHEM
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