Atomic layer deposition technology and method used for preparing iridium thin film
An atomic layer deposition and thin film technology, applied in coating, metal material coating process, gaseous chemical plating, etc., can solve the problems of blocked valve and high production cost, achieve easy operation, good step coverage, good deposition process Effect
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Embodiment 1
[0029] A kind of with 1-ethylcyclopentadienyl-1 as liquid iridium source precursor, with anhydrous hydrazine reducing agent as the iridium thin film atomic layer deposition method of reducing precursor, comprising the following steps:
[0030] S1. Use atomic layer deposition equipment to heat 1-ethylcyclopentadienyl-1 liquid iridium source raw material to 120°C, and evacuate to the ultimate pressure, and the ultimate pressure after evacuation is 0.5Pa;
[0031] S2. After the atomic layer deposition system is heated evenly, the heating time is 40 minutes, and then the carrier gas flow rate is turned on to 20 sccm. The uniform heating temperature of the atomic layer deposition system is 200 ° C, and the pressure in the atomic layer deposition system is 30 Pa;
[0032] S3, open the 1-ethylcyclopentadienyl-1 liquid iridium source atomic layer deposition pulse valve, the pulse valve opening time is 1000ms, so that the 1-ethylcyclopentadienyl-1 liquid iridium source is introduced int...
Embodiment 2
[0039] A kind of 3-cyclohexadienyl as liquid iridium source precursor, the iridium thin film atomic layer deposition method as reducing precursor with methylhydrazine reducing agent, comprises the following steps:
[0040] S1. Use atomic layer deposition equipment to heat the 3-cyclohexadiene-based liquid iridium source material to 130°C, and vacuumize to the ultimate pressure. The ultimate pressure after vacuuming is 0.5Pa;
[0041]S2. After the atomic layer deposition system is heated evenly, the heating time is 40 minutes, and then the carrier gas flow rate is turned on at 50 sccm. The uniform heating temperature of the atomic layer deposition system is 300°C, and the pressure in the atomic layer deposition system is 80Pa;
[0042] S3. Open the 3-cyclohexadiene-based liquid iridium source atomic layer deposition pulse valve, and the pulse valve opening time is 2000ms, so that the 3-cyclohexadiene-based liquid iridium source is introduced into the reaction chamber of the equi...
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