A kind of tackifier for sealing grease, preparation method and application
A sealing grease and tackifier technology, which is applied in additives, petroleum industry, lubricating compositions, etc., can solve the problems of low temperature resistance and thickening effect of shield tail sealing grease, high production cost, poor low temperature resistance, etc. , to achieve the effect of solving the problem that the low temperature resistance performance and the thickening effect cannot be equal, the product performance is stable, and the low temperature resistance performance is improved
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Embodiment 1
[0028] A kind of preparation method of tackifier for sealing grease is as follows:
[0029] First, put 10 # Pour 3000g of base oil into the reactor at a constant speed, turn on the stirring frequency of 10HZ, and heat up to 100°C;
[0030] Then, divide polymethacrylate FILB82390g and EVA200g into three parts on average, pour them into the reaction kettle three times, with an interval of 10 minutes each time, and then rapidly heat up to 130°C-160°C at a stirring frequency of 20HZ;
[0031] Then adjust the stirring frequency to 30HZ, and keep the temperature constant for 1.5 hours;
[0032] Finally, pour 45g of T551 into the reaction kettle at a constant speed, adjust the stirring frequency to 40HZ, and stir at a constant temperature for 1-2 hours to obtain a new type of thickener.
[0033] The kinematic viscosity and pour point of the prepared tackifier and polyisobutylene 2400 were compared, and the specific results are shown in Table 1.
[0034] Table 1. Performance parame...
Embodiment 2
[0037] A kind of preparation method of tackifier for sealing grease is as follows:
[0038] First, the 25 # Pour 3000g of base oil into the reactor at a constant speed, turn on the stirring frequency of 10HZ, and heat up to 100°C;
[0039] Then, divide the polymethacrylate FILB82470g and EVA210g into three parts, pour them into the reaction kettle three times, with an interval of 10 minutes each time, and then rapidly heat up to 130°C-160°C at a stirring frequency of 20HZ;
[0040] Then adjust the stirring frequency to 30HZ, and keep the temperature constant for 1 hour;
[0041] Finally, pour 70g of T551 into the reaction kettle at a constant speed, adjust the stirring frequency to 40HZ, and stir at a constant temperature for 2-3 hours to obtain a new type of thickening material.
[0042] The kinematic viscosity and pour point of the prepared tackifier and polyisobutylene 2400 were compared, and the specific results are shown in Table 2.
[0043] Table 2. Performance parame...
Embodiment 3
[0046] A kind of preparation method of tackifier for sealing grease is as follows:
[0047] First, pour 3000g of 650SN base oil into the reaction kettle at a constant speed, turn on the stirring frequency of 10HZ, and heat up to 100°C;
[0048] Then, divide polymethacrylate FILB72320g, polymethacrylate FILB8280g and EVA240g into three parts on average, and pour them into the reaction kettle three times, with an interval of 10 minutes each time, and then rapidly heat up to 130°C at a stirring frequency of 20HZ- 160°C;
[0049] Then adjust the stirring frequency to 30HZ, and keep the temperature constant for 1 hour;
[0050] Finally, pour 45g of diphenylamine into the reaction kettle at a constant speed, adjust the stirring frequency to 40HZ, and stir at a constant temperature for 2-3 hours to obtain a new type of thickening material.
[0051] The kinematic viscosity and pour point of the prepared tackifier and polyisobutylene 2400 were compared, and the specific results are s...
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