Lubricant composition for fluid dynamic bearing
A technology of lubricating oil composition and fluid bearing, applied in the direction of lubricating composition, petroleum industry, base material, etc., can solve the problems of easy hydrolysis, corrosion of metal materials, etc., achieve low evaporation, low viscosity characteristics, good low temperature fluidity Effect
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[0213] Next, the present invention is further described in detail through examples, but the present invention is not limited by these examples.
[0214] Various properties of lubricating oils were measured according to the following methods.
[0215] (1) Kinematic viscosity
[0216] Measured at -100°C and -20°C according to JIS K2283.
[0217] (2) Viscosity index
[0218] Measurement was performed in accordance with JIS K2283.
[0219] (3) Pour point
[0220] Measurement was performed in accordance with JIS K2269.
[0221] (4) Evaporation loss
[0222]According to the thermal stability test of JIS C201, the evaporation loss amount was measured at 120 degreeC and heat-processing for 24 hours.
[0223] (5) Hydrolysis test
[0224] Put 75g of sample oil, 25g of distilled water and weighed copper catalyst into a glass bottle, seal it, and rotate the glass bottle in a constant temperature tank at 93°C for 48 hours, then measure the mass loss of the copper catalyst and the to...
preparation example 1
[0230] 300 g of 2-hexyldecanol, 300 g of 1-bromodecane, 30 g of tetrabutylammonium bromide, and 500 g of 30% by mass sodium hydroxide aqueous solution were charged into a 2-liter glass flask, and stirred and reacted at 50° C. for 20 hours.
[0231] After the reaction, the reaction mixture was transferred to a separatory funnel, the aqueous phase was removed by filtration, and the remaining organic phase was washed 5 times with 500 ml of water.
[0232] 2-Hexyldecyldecyl ether was isolated from the organic phase by distillation under reduced pressure.
[0233] Next, using branched eicosanol obtained from the dimer of decene and 2-hexyldecanol and 2-octyldodecanol obtained by the Guerbet reaction, branched eicosanol was obtained by a similar reaction. Alkyl butyl ether, 2-hexyl decyl nonyl ether, 2-octyl dodecyl pentyl ether, 2-octyl dodecyl hexyl ether.
preparation example 2
[0235] 317g of 3,5,5-trimethylhexanol, 216g of 1,4-dibromobutane, 14.3g of tetrabutylammonium bromide, and 442g of 52% by mass sodium hydroxide aqueous solution were charged into a 2-liter glass flask , and stirred the reaction at 70 °C for 8 hours.
[0236] After the reaction, the reaction mixture was transferred to a separatory funnel, the aqueous phase was removed by filtration, and the remaining organic phase was washed 5 times with 500 ml of water.
[0237] 1,4-Bis(3,5,5-trimethylhexyloxy)butane was separated from the organic phase by distillation under reduced pressure.
[0238] Below, using 3,5,5-trimethylhexanol, 2-ethylhexanol, nonanol, decanol, 3,7-dimethyloctanol, octanol and a mixed alcohol of octanol and nonanol, by A similar reaction gives 1,5-bis(3,5,5-trimethylhexyloxy)pentane, 1,6-bis(3,5,5-trimethylhexyloxy)hexane, 1, 8-bis(3,5,5-trimethylhexyloxy)octane, 1,8-bis(2-ethylhexyloxy)octane, 1,5-bis(nonyloxy)-3- Methylpentane, 1,5-bis(decyloxy)-3-methylpentane,...
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