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A surface treatment method for friction-induced catalytic bio-oil esterification function

A friction induction and surface treatment technology, applied in chemical instruments and methods, chemical/physical processes, biofuels, etc., can solve problems such as corrosion and wear of bio-oil, enhance surface lubrication performance, improve tribological performance, and facilitate operation. Effect

Active Publication Date: 2022-07-12
HEFEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a surface treatment method for friction-induced catalytic bio-oil esterification to solve the problem of corrosion and wear of bio-oil on the material surface in situ

Method used

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  • A surface treatment method for friction-induced catalytic bio-oil esterification function
  • A surface treatment method for friction-induced catalytic bio-oil esterification function
  • A surface treatment method for friction-induced catalytic bio-oil esterification function

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] 1) The surface of the QT600 friction pair is textured by a laser marking machine, and the texture shape is processed into a long strip. The texture width is 85 μm, the texture spacing is 200 μm, the texture depth is 35 μm, and the laser marking power is 4.5 W, after texture treatment, use metallographic sandpaper to remove burrs.

[0028] 2) Disperse 4 g of polytetrafluoroethylene (PTFE) and 1 g of catalyst powder into 100 mL of anhydrous ethanol solution, use a probe-type ultrasonic processor for ultrasonic treatment for 5 min, then quickly filter out the mixed powder, and dry it at 80 °C to remove residual residues. ethanol to obtain a homogeneously mixed powder.

[0029] 3) Spread the evenly mixed powder evenly on the surface of the textured friction pair, cover with a layer of weighing paper, and load 10 MPa on the tablet press for 10 minutes to obtain a pre-pressed friction pair.

[0030] 4) Move the pre-pressed friction pair into a muffle furnace, calcine at 350 ...

Embodiment 2

[0034] 1) The surface of the QT600 friction pair is textured by a laser marking machine, and the texture shape is processed into a long strip. The texture width is 85 μm, the texture spacing is 200 μm, the texture depth is 35 μm, and the laser marking power is 4.5 W, after marking, use metallographic sandpaper to remove burrs.

[0035] 2) Disperse 3 g of polytetrafluoroethylene (PTFE) and 2 g of catalyst powder into 100 mL of anhydrous ethanol solution, ultrasonically treat with a probe-type ultrasonic processor for 5 min, then quickly filter out the mixed powder, and dry it at 80 °C to remove residual. ethanol to obtain a homogeneously mixed powder.

[0036] The remaining steps are the same as in Example 1.

[0037] Tribological test conditions are the same as Example 1. The test results are shown in Table 1: the average friction coefficient of the untreated QT600 friction pair is 0.15, and the wear rate is 4.14×10 -6 mm 3 / N*m; in this example, the tribological propertie...

Embodiment 3

[0039] 1) The surface of the friction pair coated with Ni-P coating is textured by a laser marking machine, and the texture shape is processed into a long strip with a texture width of 85 μm, a texture spacing of 200 μm, and a texture depth of 35 μm. , The laser marking power is 4.5W, and after the marking treatment, it is polished with metallographic sandpaper to remove burrs.

[0040] 2) Disperse 1.8g of polytetrafluoroethylene (PTFE) and 1.2g of catalyst powder into 100mL of anhydrous ethanol solution, ultrasonically treat it with a probe-type ultrasonic processor for 5 minutes, then quickly filter out the mixed powder, and dry it at 80 °C to remove Residual ethanol, resulting in a homogeneously mixed powder.

[0041] The remaining steps are the same as in Example 1.

[0042] The sample disc under the tribological test is the sample after the Ni-P coating treatment in this example, and other friction conditions are the same as Example 1. The test results are shown in Tabl...

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Abstract

The invention discloses a surface treatment method of friction-induced catalytic bio-oil esterification function. The catalyst is filled on the surface of friction pair through laser processing and texture filling technology, so as to realize the in-situ catalytic bio-oil esterification function in the friction process. The invention solves the problem of corrosion and wear of biological oil in situ through surface treatment. The surface treatment method is simple and easy to implement. It is not only suitable for ordinary carbon steel materials, but also can be combined with other surface treatment technologies such as surface coating, and can be widely used in the corrosion resistance and friction reduction lubrication of metal materials in the bio-oil environment. and other fields.

Description

1. Technical field [0001] The invention belongs to the technical field of material surface treatment, in particular to a surface treatment method with a friction-induced catalytic esterification function of biological oil. 2. Background technology [0002] With the rapid development of society, the demand for traditional fossil energy such as oil has increased year by year. However, the large-scale exploitation and use of fossil energy has triggered an energy crisis and a global greenhouse effect. To solve these problems, a variety of new clean and renewable energy sources have been developed to reduce the dependence on traditional fossil energy. Bio-oil is a liquid fuel obtained from biomass through pyrolysis technology, which is expected to replace traditional fossil energy and be applied to engines. Compared with traditional fossil energy sources, bio-oil has a wide range of sources, various types and large quantities of raw materials; the content of sulfur in bio-oil is...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B05D5/08B05D7/24B05D3/00B05D3/02B01J27/053B23K26/362B23K26/70
CPCB05D5/083B05D5/086B05D7/24B05D3/002B05D3/007B05D3/0272B01J27/053B23K26/362B23K26/70B05D2202/15Y02E50/10
Inventor 徐玉福彭玉斌陈星包一琛田明
Owner HEFEI UNIV OF TECH