Sound insulation material and method for preparing sound insulation material
A technology of sound insulation materials and polymer materials, applied in the field of sound insulation materials and preparation of sound insulation materials, to achieve the effect of improving the effect of noise isolation
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Embodiment 1
[0065] 1. Preparation of modified graphene materials
[0066] Add 1 g of graphene oxide with a size of 1 μm to 1 LSOCl 2 , 20ml of anhydrous DMF, reflux at 80°C for 20h, filter and wash to obtain graphene oxide acid chloride.
[0067] Inject 100ml of anhydrous THF into a round bottom bottle under nitrogen protection, then add 2.5g of 4-hydroxy-2,2,6,6-tetramethylpiperidine nitroxide radical, 1.6g of p-dimethylaminopyridine and mix well . Then add 1 g of graphene oxide acid chloride, and react under reflux at 75 degrees Celsius for 48 hours. After filtering and washing, drying is used to obtain a graphene initiator.
[0068] Under the protection of argon, the purified 0.15g CuBr, 0.2g pentamethyldiethylenetriamine, 10g styrene, and 1g graphene initiator were sequentially added to 50ml anhydrous toluene. Under an argon protective atmosphere, stir and reflux at 95 degrees Celsius for 4 days to obtain a pre-modified graphene solution.
[0069] Add 1 g of (3-epoxypropyl)trimet...
Embodiment 2
[0073] The method for preparing the modified graphene material in this example and the process parameters for preparing the sound-insulating material are the same as those in Example 1, except that the size of the graphene used is 5 microns.
Embodiment 3
[0075] The method for preparing the modified graphene material in this embodiment and the process parameters for preparing the sound-insulating material are all the same as in Example 1. The difference is that the addition of the modified graphene material is 100g, the addition of polypropylene is 900g, and the honeycomb honeycomb core The hypotenuse length c is 8mm.
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