Dental whitening and degerming coating material and preparation method and application thereof

A coating material and whitening technology, used in tooth protection coatings, dental preparations, dentistry, etc., can solve problems such as tooth surface damage, stimulation of oral mucosa, and limited whitening effect.

Pending Publication Date: 2021-04-13
XIAN UNIV OF POSTS & TELECOMM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to overcome the above-mentioned shortcoming of the prior art, provide a kind of dental whitening antibacterial coating material and its preparation m

Method used

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  • Dental whitening and degerming coating material and preparation method and application thereof
  • Dental whitening and degerming coating material and preparation method and application thereof
  • Dental whitening and degerming coating material and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0029] The preparation method of the dental whitening and antibacterial coating material comprises the following steps:

[0030] (1) Mix the powder materials in proportion, SiO 2 , The mass sum of piezoelectric materials and additives is 100%.

[0031] (2) Mill the material obtained in step (1) at high speed in a ball mill to obtain a mixture. The milling speed is 800-2000r / min, preferably 1000-1500r / min, and the milling time is 2-16h, preferably 10-16h.

[0032] (3) mixing the mixture obtained in step (2) with the blending liquid to obtain a paste material; the blending liquid is used as a mixture dispersion to improve adhesion, and is composed of glycerin, water and povidone K30, and the mass ratio It is (2-4): (3-5): (1-4), preferably 4:5:1; the mass ratio of the mixture to the blended liquid is (2-3): (1-2), preferably 2: 1;

[0033] (4) Apply the paste material obtained in step (3) to the outside of the dental restoration matrix, completely wrap the dental restoration ...

Embodiment 1

[0036] (1) According to the content of the ingredients shown in Table 1, take the required raw material ingredients and mix them thoroughly and evenly.

[0037] Table 1 example 1 material content formula

[0038] components Mass content wt% SiO 2

70 al 2 o 3

3 K 2 o

4 CeO 3 ZrO 5 P 2 o 5

5 BaTiO 3

10

[0039] (2) Ball mill the mixed material for 16 hours at a rotating speed of 800r / min to obtain a well-mixed and well-dispersed mixture.

[0040] (3) Blend the obtained mixed powder with the blending solution at a mass ratio of 2:1 to prepare a paste material. The blending solution is composed of glycerol, water and povidone K30 in a mass ratio of 4:5:1.

[0041] The resulting paste was coated on the surface-treated base of the metal-ceramic dental restoration, and was cured at 770°C for 20 minutes.

[0042] A dental restoration with whitening and antibacterial functions is obtained.

[0043] f...

Embodiment 2

[0045] (1) According to the content of the ingredients shown in Table 2, take the required raw material ingredients and mix them thoroughly and evenly.

[0046] Table 2 example 2 material content formula

[0047]

[0048]

[0049] (2) Ball mill the mixed material for 12 hours at a rotational speed of 1000 r / min to obtain a mixed powder material with uniform mixing and good dispersibility.

[0050] (4) Blend the obtained mixed powder with the blending solution at a mass ratio of 3:1 to prepare a paste material. The blending solution is composed of glycerol, water and povidone K30 in a mass ratio of 4:5:1.

[0051] (3) Apply the obtained paste on the base of the all-ceramic dental restoration after surface treatment, and heat it at 800° C. for 15 minutes to solidify to obtain a dental restoration with whitening and sterilization functions.

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Abstract

The invention discloses a dental whitening and degerming coating material and a preparation method and application thereof. The coating material is composed of SiO2, an additive and a piezoelectric material. A dental prosthesis with the surface layer containing the piezoelectric material is prepared by coating and curing the surface layer of the dental prosthesis, and SiO2 serves as a main material and can activate the piezoelectric property of the material due to pressure changes under the action of external force such as vibration and friction in daily life due to the piezoelectric material, so that a large number of active groups are generated. Research shows that the active groups generated by the piezoelectric effect can effectively remove stains on the surfaces of teeth and remarkably whiten the teeth, no side effect exists, enamel and oral mucosa cannot be damaged, and then the self-whitening and degerming functions of the teeth are achieved through the piezoelectric effect on the surfaces of the teeth in the chewing and tooth brushing process.

Description

【Technical field】 [0001] The invention belongs to the technical field of teeth whitening and repairing, and in particular relates to a dental whitening and antibacterial coating material and its preparation method and application. 【Background technique】 [0002] In the field of stomatology, with the improvement of public aesthetic requirements, dental restoration materials must not only meet good biocompatibility and excellent mechanical properties, but also have good optical properties to meet the aesthetics of the restoration. [0003] Teeth whitening is an important aspect of oral aesthetics. At present, teeth whitening is mainly achieved through abrasives or whitening agents. Abrasives are used to remove stains and stains on the surface of teeth by grinding. This method is a physical action method. Abrasives often have relatively high hardness. Therefore, with the increase in the number of grinding times, certain damages will inevitably be caused on the tooth surface, a...

Claims

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Application Information

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IPC IPC(8): A61K6/20A61K6/15A61K6/831A61K6/802A61K6/818A61K6/838A61K6/829A61K6/833
CPCA61K6/20A61K6/15A61K6/831A61K6/802A61K6/818A61K6/838A61K6/829A61K6/833
Inventor 张亚明李仃徐建刚张云光贾艳敏任卫姚国光顾生越
Owner XIAN UNIV OF POSTS & TELECOMM
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