Lithium battery cell restoring method using heat treatment, and lithium battery cell manufacturing method including same
A lithium battery, high temperature treatment technology, applied in the direction of electrolyte battery manufacturing, lithium battery, electrical components, etc., can solve problems such as loss of capacity
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preparation example
[0067] Manufacture of cathode
[0068] 0.5Li to be used as positive electrode active material2 MnO 3 0.5Li(Ni 0.45 mn 0.35 Ni 0.20 )O 2 , conductive material (carbon black, carbon black) and binder (PVdF) were added to NMP (N-methyl-2-pyrrolidone, N-methyl-2-pyrrolidone) with a weight ratio of 90:5:4, and carried out mixed to prepare a positive electrode mixture.
[0069] The prepared positive electrode mixture was coated on a 20 μm thick aluminum foil with a thickness of 80 μm, and then rolled and dried to manufacture a positive electrode.
[0070] Manufacture of negative electrode
[0071] Artificial graphite used as negative electrode, conductive material (carbon black, carbon black), conductive material (carbon black, carbon black) and binder (PVdF) were added to NMP (N-methyl -2-pyrrolidone, N-methyl-2-pyrrolidone), and mixed to prepare the negative electrode mixture.
[0072] The prepared negative electrode mixture was coated on a 20 μm thick copper foil with...
example 1
[0076] The process of charging the lithium battery cell prepared in Preparation Example at 0.33C to 4.2V and discharging at 1.0C to 2.5V was repeated to measure changes in capacity and voltage according to the progress of the cycle.
[0077] exist figure 1 Results for up to 40 cycles are shown in .
[0078] refer to figure 1 , it can be seen that as the cycling progresses, the changes in capacity and voltage move along the direction of the arrows, so that the overvoltage increases and the capacity decreases.
Embodiment 1
[0080] While repeating the process of charging the lithium battery cell prepared in Preparation Example at 0.33C to 4.2V and discharging at 1.0C to 2.5V in a chamber at 25°C, the discharge was measured with a charge / discharge device of PNE Corporation capacity. When the discharge capacity reached about 90% of the initial discharge capacity (degradation rate: 10%, 40 cycles), the cycle was stopped. The battery cell was subjected to a high-temperature treatment at 80° C. for 6 hours in a state where the SOC was 0.
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