Anti-aging self-flame-retardant hyperbranched fluorine-containing polyacrylate emulsion and preparation method thereof
A kind of polyacrylate emulsion, flame retardant technology, applied in the field of hyperbranched polymer synthesis
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Embodiment 1
[0030] An anti-aging self-flame-retardant hyperbranched fluorine-containing polyacrylate emulsion, comprising the following raw materials in parts by mass:
[0031]
[0032]
[0033] A preparation method of anti-aging self-flame-retardant hyperbranched fluorine-containing polyacrylate emulsion, comprising the following steps:
[0034] S1: Mix DMAP, HOAT, and p-toluenesulfonic acid-doped polyaniline uniformly at a mass ratio of 1:0.6:1.5 to prepare a catalyst;
[0035] S2: Preparation of modified layered double metal hydroxide:
[0036] i: Intercalation modification: Add Mg / Al type layered double metal hydroxide to an aqueous solution with a mass fraction of 5-10% dodecylguanidine hydrochloride, control the solid-liquid ratio to 1g / 10mL, and perform ultrasonic treatment After 0.5h, filter and dry to obtain guanidine-modified layered double hydroxides;
[0037] ii: Functional modification: Dissolve phenyl salicylate, light stabilizer 622, and vinyltrimethoxysilane in eth...
Embodiment 2
[0042] An anti-aging self-flame-retardant hyperbranched fluorine-containing polyacrylate emulsion, comprising the following raw materials in parts by mass:
[0043]
[0044]
[0045] A preparation method of anti-aging self-flame-retardant hyperbranched fluorine-containing polyacrylate emulsion, comprising the following steps:
[0046] S1: Mix DMAP, HOAT, and p-aminobenzenesulfonic acid-doped polyaniline uniformly at a mass ratio of 1:0.8:1.75 to prepare a catalyst;
[0047] S2: Preparation of modified layered double metal hydroxide:
[0048] i: Intercalation modification: Add nano-Ni / Al type layered double metal hydroxide to an aqueous solution with a mass fraction of 7.5% dodecylguanidine acetate, control the solid-liquid ratio to 1g / 12.5mL, and ultrasonically treat After 1.5h, filter and dry to obtain guanidine-modified layered double hydroxides;
[0049] ii: Functional modification: Dissolve phenyl salicylate, light stabilizer 783, and vinyltrimethoxysilane in ethan...
Embodiment 3
[0054] An anti-aging self-flame-retardant hyperbranched fluorine-containing polyacrylate emulsion, comprising the following raw materials in parts by mass:
[0055]
[0056] A preparation method of anti-aging self-flame-retardant hyperbranched fluorine-containing polyacrylate emulsion, comprising the following steps:
[0057] S1: Mix DMAP, HOAT, and phosphotungstic acid-doped polyaniline uniformly at a mass ratio of 1:1:2 to prepare a catalyst;
[0058] S2: Preparation of modified layered double metal hydroxide:
[0059] i: Intercalation modification: add nano-Mn / Fe layered double metal hydroxide to an aqueous solution with a mass fraction of 10% polyhexamethylene biguanide, control the solid-liquid ratio to 1g / 15mL, sonicate for 2h, and filter , drying to obtain guanidine modified layered double metal hydroxides;
[0060] ii: Functional modification: Dissolve phenyl salicylate, light stabilizer 944, and vinyltrimethoxysilane in ethanol according to the dosage ratio of 1g...
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