High-pressure strain device and preparation method of high-pressure reinforced metal
A high pressure, pressure cavity technology, applied in the field of material processing, can solve problems such as single axial force
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Embodiment 1
[0066] Cutting and annealing the high-purity aluminum column in sequence to obtain oblique round high-purity aluminum column (mass fraction 99.999%), the angle of inclination is 30°. according to figure 1 Assembly method Install the oblique cylindrical high-purity aluminum column in the sample chamber 152 and perform high-pressure deformation. First, increase the pressure for 10 minutes, then maintain the pressure at a pressure of 0.5 GPa for 30 minutes, and then release the pressure for 10 minutes to obtain a high-pressure sample with a deformation degree of 22%. Pure aluminum column, take out the deformed high-purity aluminum column and grind and polish it.
[0067] figure 2 Metallographic diagrams of high-purity aluminum samples before and after high-pressure deformation. The metallographic diagram obtained by observing the microstructure of the high-purity aluminum column without high-pressure deformation, the observation result is figure 2 In figure a in the middle, ...
Embodiment 2
[0070] The difference between Example 2 and Example 1 is that the pressure is 1.5 GPa, a high-purity aluminum column with a deformation degree of 54% is obtained, and the deformed high-purity aluminum column is taken out and polished.
[0071] The metallographic diagram obtained by observing the microstructure of a high-purity aluminum column with a deformation degree of 54% after grinding and polishing, the observation result is figure 2 Figure c, from figure 2 middle a map and figure 2 From the comparison in c, it can be seen that the metallographic structure size of the high-pressure pure aluminum sample prepared in the example of the present invention is obviously smaller than the metallographic structure size of the pure aluminum sample annealed before high pressure.
[0072] The microhardness test was carried out on the high-purity aluminum column with a degree of deformation of 54% after high-pressure strain in Example 2. The test results showed that the microhardne...
Embodiment 3
[0074] The difference between Example 3 and Example 1 is that the pressure is 2 GPa, a high-purity aluminum column with a deformation degree of 68% is obtained, and the deformed high-purity aluminum column is taken out and polished.
[0075] The metallographic diagram obtained by observing the microstructure of a high-purity aluminum column with a deformation degree of 68% after grinding and polishing, the observation result is figure 2 Middle d figure, from figure 2 middle a map and figure 2 From the comparison in figure d, it can be seen that the metallographic structure size of the high-pressure pure aluminum sample prepared in the example of the present invention is obviously smaller than the metallographic structure size of the pure aluminum sample annealed before high pressure.
[0076] The microhardness test was carried out on the high-purity aluminum column with a degree of deformation of 68% after high-pressure strain in Example 3. The test result shows that the m...
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