A Tibetan Codonopsis compound composition with anti-allergic and soothing effects, its preparation method and application
A technology of Tibetan Codonopsis compound prescription and composition, applied in the field of Tibetan Codonopsis compound prescription composition and preparation thereof, can solve the problems of high price, poor water solubility, single effect and the like
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Embodiment 1
[0026] This embodiment provides a tibied part of the Tibetan Participation Composition with anti-sensitivity, including the following weight materials: 40 parts of the Tibetan Party, 30 collisants and 30 yellow squid.
[0027] The preparation method of the composition includes the following steps:
[0028] (1) According to the proportion of dry Tibetan Participation, Heluslaus and Huang Shiihua, mix, smash, over 20 mesh sieve; then add 15 times of the mass fraction of 70% ethanol, reflux extraction 2 times, each time The filtrate was combined after filtration, and ethanol was recovered under reduced pressure under 65 ° C.
[0029] (2) Add 15 times hot water of the immersion paste to the extract from the step (1), and the stirring is uniform, and 12 h is placed;
[0030] (3) The material obtained by step (2) was centrifuged at 4000 rpm to 20 min, discarded, taking the supernatant, concentrated atmospheric pressure, and dried under 60 ° C, pulverized, and the composition was obtaine...
Embodiment 2
[0032] This embodiment provides a Tibetan Participant Composition with anti-sensitive soothing, including the following weight materials: 10 copies of the Tibetan Party, 35 complicss and 50 parts of Huang Shunxi.
[0033] The preparation method of the composition includes the following steps:
[0034] (1) According to the proportion of dry Tibetan Participation, Heluslaus and Huang Shiihua, mix, smash, over 20 sieve; then add 20 times the mass fraction of the medicinal material to 30% ethanol, reflow extraction 1 time, extraction time It was 3 h, filtrate, and the ethanol was recovered under reduced pressure at 75 ° C.
[0035] (2) Add 20-fold hot water from the immersion paste obtained by step (1), and uniformly disperse and disperse, place 24 h;
[0036] (3) The material obtained from step (2) was centrifuged at 5000 rpm to 30 min, discarded the precipitate, taking the supernatant, concentrated at normal pressure, and dried under vacuum under 70 ° C, and pulverized.
Embodiment 3
[0038] This embodiment provides a composition of a Tibetan Participant Composition with Anti-sensitive Soothing, including 40 copies of the following weight: 40 copies of the Tibetan ginseng, 50 collisants and 10 yellow squid.
[0039] The preparation method of the composition includes the following steps:
[0040] (1) According to the proportion of dry Tibetan Participation, Heluslaus and Huang Shiki flower medicinal materials, mix, smash, over 20 mesh sieve; then add 5 times the mass fraction of the medicinal material is 90% ethanol, reflux extraction 3 times, each After 1 h, after filtration, the filtrate was combined, and ethanol was recovered under reduced pressure under 55 ° C.
[0041] (2) Add 5 times hot water of the immersion paste to the immersion paste obtained by step (1), and the stirring dispersion is uniform, and 12 h is placed;
[0042] (3) The material obtained by step (2) was centrifuged at 3000 rpm to 15 min, discarded, taking the supernatant, concentrated at no...
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