Coating composition with easy-to-clean performance
A composition and coating technology, applied in polyester coatings, coatings, etc., can solve problems such as low compatibility and difficulty in finding solvents
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Embodiment 1
[0074] Embodiment 1: the preparation of polyester
[0075] A mixture of 0.1 parts of dibutyltin dilaurate, 33.3 parts of diglyme, 26.8 parts of Fluorolink E10H, and 6.7 parts of TMA was added to the reactor, stirred and heated to 120°C under a nitrogen atmosphere. The reaction was allowed to proceed until the solution was clear. 21.6 parts of Cardura E10P were added to the reaction mixture and the temperature was raised to 130°C. The reaction was allowed to proceed until the acid number was below 8 mg KOH / g. 11.5 parts of ε-caprolactone were added to the reactor and the temperature was raised to 160°C. The reaction was allowed to proceed for 4 hours, after which time the reaction mixture was cooled to 50 °C.
[0076] The resulting polyester has an M of 3768 n , based on solids, an acid value of 8 mg KOH / g or less and an OH value of 59.6 mg KOH / g. The solids content of the solution was 66.6% by weight.
Embodiment 2
[0077] Embodiment 2: the preparation of coating composition
[0078] Three coating compositions have been prepared using the polyester synthesized in Example 1 as an additive present in amounts of 0% (comparative), 0.5% by weight and 1% by weight. The amounts are given in Table 1 in parts by weight.
[0079] Table 1
[0080] 0% additives 0.5% additive 1% additive base resin Resin 3261 68 68 68 hardener Cymel 303 12 12 12 catalyst p-Toluenesulfonic acid 0.2 0.2 0.2 pigment cobalt chromite 8 8 8 filler TiO 2
Embodiment 3
[0081] Example 3: Coated panels
[0082] Coat panel AZ100 (zinc / aluminum alloy coated steel) to a dry film thickness of 5 μm with the commercially available Cr-free primer APW9R406445 from AkzoNobel first by passing RDS 12" coat thickness wire. Pass RDS 22" coat thickness Wires The coating composition prepared in Example 2 was applied as a topcoat to a dry film thickness of 15 μm. The panel was then baked in an oven at 270°C for 33 sec, at a peak metal temperature of 232°C.
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