Controlled synthesis process of functionalized ordered macroporous (less than or equal to 1mm) graphite rotor for aluminum alloy refining

A technology of graphite rotor and synthesis process, applied in additive processing, additive manufacturing, etc., can solve the problems of low hydrogen removal efficiency, large bubble diameter, etc., and achieve the effects of improving pass rate, eliminating thermal stress, and preventing cracking

Pending Publication Date: 2022-07-22
LIUZHOU VOCATIONAL & TECHN COLLEGE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, limited by the existing processing technology level, it is extremely difficult to process nozzles with a diameter of ≦1mm on a graphite rotor...

Method used

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  • Controlled synthesis process of functionalized ordered macroporous (less than or equal to 1mm) graphite rotor for aluminum alloy refining
  • Controlled synthesis process of functionalized ordered macroporous (less than or equal to 1mm) graphite rotor for aluminum alloy refining
  • Controlled synthesis process of functionalized ordered macroporous (less than or equal to 1mm) graphite rotor for aluminum alloy refining

Examples

Experimental program
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Effect test

Embodiment 1

[0128] Embodiment 1 of the present invention provides a control synthesis process for a functionalized ordered macroporous (≦1mm) graphite rotor for aluminum alloy refining, which includes the following steps:

[0129] In step S1, the hole-making template 100 is provided, and the hole-making template 100 is formed by 3D printing technology. Specifically, the hole-making template 100 may include the following steps:

[0130] Step S11, according to the size parameters of the graphite rotor to be fabricated, determine the size parameters of the hole-making template 100, specifically, it includes the following steps:

[0131] Determine the overall size of the graphite rotor blank according to the final size parameters of the graphite rotor: specifically, according to the graphite rotor diameter D 1 and the overall height H of the graphite rotor 1 Wait( figure 2 ), and increase the corresponding machining allowance D' and height allowance H' on the surface of each outline of the...

Embodiment 2

[0159] Embodiment 2 of the present invention provides a controlled synthesis process of a functionalized ordered macroporous (≦1mm) graphite rotor for aluminum alloy refining, comprising the following steps:

[0160] Step S1, providing a hole-making template 100: the structure of the hole-making template 100 is the same as that of Embodiment 1, and is not repeated here for the sake of omission of space. The hole-making template 100 is formed by 3D printing technology, which may specifically include the following steps:

[0161] Step S11, according to the size parameters of the graphite rotor to be fabricated, determine the size parameters of the hole-making template 100, specifically, it includes the following steps:

[0162] Determine the overall size of the graphite rotor blank according to the final size parameters of the graphite rotor: according to the diameter D of the graphite rotor 1 and the overall height H of the graphite rotor 1 Wait( figure 2 ), increase the co...

Embodiment 3

[0190] Embodiment 3 of the present invention provides a control synthesis process for a functionalized ordered macroporous (≦1mm) graphite rotor for aluminum alloy refining, which includes the following steps:

[0191] In step S1, a hole-making template 100 is provided, and the structure of the hole-making template 100 is the same as that of Embodiment 1, and is not repeated here for the sake of omission of space. The hole-making template 100 is formed by 3D printing technology, which may specifically include the following steps:

[0192] Step S11, according to the size parameters of the graphite rotor to be fabricated, determine the size parameters of the hole-making template 100, specifically, it includes the following steps:

[0193] Determine the overall size of the graphite rotor blank according to the final size parameters of the graphite rotor: according to the diameter D of the graphite rotor 1 and the overall height H of the graphite rotor 1 Wait( figure 2 ), add ...

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Abstract

The invention provides a controlled synthesis process of a functionalized ordered macroporous (less than or equal to 1mm) graphite rotor for aluminum alloy refining, which comprises the following steps of: providing a pore-forming template, filling coke powder and the pore-forming template into a mold sheath, and performing isostatic pressing to obtain a rotor blank; the rotor blank is put into a roasting furnace to be sintered, and the rotor blank is converted into a carbonized composite material; putting the carbonized composite material into a graphitization furnace for graphitization sintering, so that the carbonized composite material is converted into a graphite composite material; and dipping the graphite composite material in a corrosive liquid to remove the annular hollow-out body made of the metal material and the branches made of the metal material. According to the preparation method, the graphite composite material with an ordered macroporous (less than or equal to 1mm) structure can be prepared, and on the basis, the functionalized graphite composite material is applied to development of a graphite rotor with a small nozzle aperture (less than or equal to 1mm), so that the bottleneck of the level of the prior art is broken through, and the quality of an aluminum melt is further improved.

Description

technical field [0001] The invention relates to a preparation technology of a novel graphite composite material, in particular to a controlled synthesis process of a functionalized ordered macroporous (≤1mm) graphite rotor for aluminum alloy refining. Background technique [0002] High-purity dense graphite material has the advantages of excellent high temperature mechanical properties, good thermal shock resistance and corrosion resistance, so it has been widely used in metallurgy and other fields. For example, in the aluminum processing industry, high-purity and dense graphite materials are generally used to prepare graphite rotors with regular pore structure, which are used as key components of hydrogen removal devices to purify aluminum melts. [0003] The effect of graphite rotor for purifying aluminum melt mainly depends on its internal pore structure and pore size, etc. This is because the reasonably distributed pore structure can effectively avoid the gas flux (N 2 ...

Claims

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Application Information

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IPC IPC(8): C22B9/05C22C1/02B22F10/28B33Y10/00B33Y80/00
CPCC22B9/05C22C1/026B22F10/28B33Y10/00B33Y80/00
Inventor 楼华山纪红伟赵冬冬陈文勇陈冬玲李宏军王大红冯艺莫文锋吴坤陈华关来德高茂涛龚荣李海安思常红李骏鹏李杨汤耀年阙燚彬刘光浩周艳李丽
Owner LIUZHOU VOCATIONAL & TECHN COLLEGE
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