Process and system for preparing low-carbon olefin from methanol or dimethylether
A process method and technology of low-carbon olefins, applied in the direction of hydrocarbon production from oxygen-containing organic compounds, chemical recovery, organic chemistry, etc., can solve the problems that cannot meet the rapid separation of gas and solid, and achieve short gas-solid residence time, equipment and particle The effect of less wear and lower difficulty
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Embodiment 1
[0029] The reaction is carried out in a gas-solid co-current downward circulating fluidized bed reactor. The feed is dimethyl ether, the feed is in liquid phase, the catalyst is SAPO34, the reactor temperature is 460°C, the regenerator temperature is 510°C, the residence time is 10 seconds, the catalyst-to-oil ratio is 30, and the reaction is performed at 0.01 MPa. The conversion rate of dimethyl ether is 99%. In the hydrocarbon products, ethylene accounts for 60%, propylene accounts for 25%, butene accounts for 8%, and the yield of low-carbon olefins is 93. %.
Embodiment 2
[0031] The reaction is carried out in a gas-solid co-current downward circulating fluidized bed reactor. The feed is dimethyl ether, gas phase feed, SAPO34 is used as the catalyst, the reactor temperature is 530°C, the regenerator temperature is 650°C, the residence time is 5 seconds, the catalyst-to-oil ratio is 18, and the reaction is carried out under normal pressure. The conversion rate of dimethyl ether is 99%. In the hydrocarbon products, ethylene accounts for 63%, propylene accounts for 24%, butene accounts for 7%, and the yield of low-carbon olefins is 95%. %.
Embodiment 3
[0033]The reaction is carried out in a gas-solid co-current downward circulating fluidized bed reactor. The feed is a mixture of dimethyl ether and water, gas phase feed, the catalyst is SAPO34, the molar ratio of dimethyl ether to water is 1:0.5, the reactor temperature is 650℃, the regenerator temperature is 780℃, and the residence time is 0.2 Second, the agent-oil ratio is 5, and the reaction is conducted at 0.95MPa. The conversion rate of dimethyl ether is 99%. In the hydrocarbon products, the proportion of ethylene is 62%, propylene is 24%, butene is 7%, and the yield of the product low-carbon olefin is 94%.
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