Stretchable liquid crystal polymer composition
A technology of polymers and mixtures, applied in the direction of synthetic resin layered products, types of packaging items, special packaging items, etc., which can solve the problems of not being able to stretch smoothly, not having instructions, and not being able to use barrier layers.
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Embodiment 1-31
[0086] To a three-necked cylindrical flask equipped with a stainless steel "c" stirrer, inlet tube, thermocouple, distillation trap, and Vigreux fractionating column connected to the condenser and receiver was added the following materials:
[0087] 372.6 g parabens,
[0088] 451.2 g of 6-hydroxy-2-naphthoic acid,
[0089] 124.2 g m-hydroxybenzoic acid,
[0090] 623.7 grams of acetic anhydride (1 mole percent excess) and
[0091] 0.06 grams of potassium acetate (30 ppm).
[0092] The flask was evacuated, flushed with dry nitrogen to remove oxygen, and then buried in an electrically heated fluidized sand bath. Heat the contents of the flask to about 150° C. while stirring at 75 rpm to acetylate the hydroxyl groups in the contents. The temperature was then raised from 150°C to 220°C over 70 minutes to distill the by-product acetic acid. Polymerization was started at 220°C and the bath temperature was raised to 320°C over 110 minutes. The acetic acid generated at this time ...
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