New alginate monoclone antiboeg and its preparation method and use
A technology of monoclonal antibody and alginate, which is applied in the direction of anti-bacterial immunoglobulin, cells modified by introducing foreign genetic material, fusion cells, etc. It can solve the problems of lack of in-depth research reports and difficulties in the means of biological effects of alginate, etc. question
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Embodiment 1
[0023] Example 1 Preparation of immunogen: Alginate cross-linked with BSA
[0024] Precisely weigh 5.0 mg of alginate and dissolve in 0.05M 50ml of boric acid buffer at pH 10, add EDCI100mg under a magnetic stirrer and react at room temperature for 8 hours, then add 0.05M 5.0ml of boric acid buffer at pH 10 to dissolve BSA, and react at room temperature for 8 hours Dialyze overnight at 4°C. EDCI should be freshly prepared.
Embodiment 2
[0025] Example 2 Animal Immunization
[0026] The immunogen prepared as in Example 1, that is: the alginate-BSA complex was dissolved in physiological saline, mixed with an equal volume of Freund's complete adjuvant, and BALB / C mice (male, six-week-old, 18-20 g , provided by the Animal Center of Chinese Academy of Medical Sciences) subcutaneously injected into the abdomen at multiple points, 40 μg / 200 μl / animal. The first booster immunization was carried out two weeks after the basic immunization, and then every 2-4 weeks, with a dose of 20μg / 200μl / bird.
[0027] One day after the initial immunization and 6 booster immunizations, the antiserum titer of the fusion mice to be taken from the spleen was measured by indirect ELISA. The normal mouse serum was used as the negative control, and the determination was carried out on the basis of (measurement well A value-blank value) / (negative control well A value-blank value)≥2.1.
Embodiment 3
[0029] Example 3 Cell Fusion
[0030] Cell fusion adopts the polyethylene glycol method: take the spleen of the mouse immunized as described in Example 2 aseptically, make a cell suspension, centrifuge, count the cells, and splenocytes (about 1 × 10 8 ) and SP2 / 0 cells (about 1×10 7 ) were mixed, centrifuged at 1000r / min for 10min, and the supernatant was removed. Place the centrifuge tube in a 37°C water bath, slowly add 1ml of 50% PEG solution (Sigma), let it stand for 1 minute, and then slowly add 9ml of serum-free culture medium IMDM. Centrifuge at 800r / min for 10min, discard the supernatant, wash twice, add complete medium to resuspend the cells for inoculation.
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