Method of extracting total flavone product from halenalin plant full flower
A technology of Caragana and total flavonoids, which is applied in the field of extracting total flavonoids from the whole flower of Caragana, can solve the problems of low output rate of total flavonoids and difficult selection of technical parameters, and achieve a reasonable extraction method, Effect of high output rate and expansion of raw material source
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[0010] Take Caragana microphylla Lam or C. intermedia Kuanget H.C. Fu as an example.
[0011] Crush the whole flowers of Caragana microphylla (or Caragana intermedia) that are naturally air-dried (or dried at a constant temperature of 50°C or 60°C), and pass through a 40-mesh (or 50-mesh or 60-mesh) sieve; weigh the sieved dry powder 1 kg, add 6-25 liters (optional 10, 15, 20 liters) 45% (or 50% or 55% or 60% or 65%) ethanol solution, 50 ℃ (or 45 ℃ or 55 ℃ or 60 ℃ or Stir and soak for 3 hours at 65° C., filter, add 4-12 liters of filter residue (optional 5, 8, 10 liters) 45% (or 50% or 55% or 60% or 65%) ethanol solution, 50 °C (or 45 °C or 55 °C or 60 °C or 65 °C) and soaked for 1 hour, extracted twice, and combined the three filtrates to obtain the upper column liquid; the upper column liquid was reduced at 60 °C (55 °C or 65 °C). Press and concentrate to reclaim ethanol until the upper column liquid has no alcohol smell; then the upper column liquid is separated through a ...
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