Method for extracting clerodendranthus spicatus
A technique of extracting kidney tea, which is applied in the field of extracting kidney tea, can solve the problems that the active ingredients of kidney tea are unstable when exposed to heat, easy to decompose, and reduce curative effect, so as to achieve less loss of active ingredients, improve curative effect, and reduce drug use. convenient effect
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[0009] Embodiment 1: take the crude product of kidney tea, remove the sundries, and break it into pieces. The kidney tea fragments were added to 3 times of water, extracted at a temperature of 40° C. for 2 hours, filtered, and the filter residue was extracted twice with 5 times of water under the same conditions, and the filtrates were combined for use. The filtrate was concentrated under reduced pressure to a density of 1.20 g / ml at a temperature of 90° C., and then spray-dried at 100° C. to obtain an extract of kidney tea. In this example, 170.0g of refined extract can be obtained per 1Kg of kidney tea raw material, and the color is tan.
Example Embodiment
[0010] Example 2: Take the crude product of kidney tea, remove foreign matter, and break it into segments. The kidney tea fragments were added to 5 times of water, extracted at a temperature of 90° C. for 2 hours, filtered, and the filter residue was extracted twice with 8 times of water under the same conditions, and the filtrates were combined for use. The filtrate was concentrated under reduced pressure to a density of 1.50 g / ml at a temperature of 90° C., and then vacuum-dried at 70° C. to obtain a kidney tea extract. In this example, 165.0g of refined extract can be obtained per 1Kg of kidney tea raw material, and the color is tan.
Example Embodiment
[0011] Embodiment 3: take the crude product of kidney tea, remove the sundries, and break it into pieces. The kidney tea fragments were added to 8 times of water, extracted at a temperature of 70° C. for 2 hours, filtered, and the filter residue was extracted twice with 3 times of water under the same conditions, and the filtrates were combined for use. The filtrate was concentrated under reduced pressure at a temperature of 90°C to a density of 1.40 g / ml, and then dried at a low temperature at 40°C to obtain the extract of kidney tea. In this example, 160.0g of refined extract can be obtained per 1Kg of kidney tea raw material, and the color is tan.
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