Nonionic associative thickener containing vinyl addition polymer backbone
An associative thickener, non-ionic technology, used in adhesive additives, polymer adhesive additives, papermaking, etc., can solve the problems of increased sedimentation of inorganic pigments or inorganic fillers
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0123] Embodiment 1: Preparation of nonionic vinyl surfactant monomer
Embodiment 11
[0125] 376.8 g of polypropylene glycol monobutyl ether (molecular weight 1000) and 400 ml of toluene were charged to a 2 liter reactor equipped with a thermometer, heating mantle, temperature regulator, overhead stirring motor, nitrogen purge and condenser with Dean-Stark trap . The reactor contents were heated to reflux under nitrogen, and residual water was removed by water / toluene azeotrope into a Dean Stark trap. Cool the contents of the reactor to 90°C, add 0.04 grams of 2,6-di-tert-butyl p-cresol, 0.4 grams of dibutyltin dilaurate and 80 grams of isocyanate α, α-dimethyl - m-isopropylbenzyl ester. The reactor contents were held at 90°C for 60 minutes and then cooled to room temperature. Toluene was removed by roto-vac to obtain the nonionic vinyl surfactant monomer of Example 1.1.
Embodiment 12
[0127] Into a 2-liter reactor equipped with a thermometer, heating mantle, temperature regulator, overhead stirring motor, nitrogen purge, and condenser with a Dean-Stark trap was charged 588 g of polypropylene glycol tridecyl ether (molecular weight 1590) and 500 mL toluene. The reactor contents were heated to reflux under nitrogen, and residual water was removed by water / toluene azeotrope into a Dean Stark trap. Cool the contents of the reactor to 90°C, add 0.04 grams of 2,6-di-tert-butyl p-cresol, 0.4 grams of dibutyltin dilaurate and 80 grams of isocyanate α, α-dimethyl - m-isopropylbenzyl ester. The reactor contents were held at 90°C for 60 minutes and then cooled to room temperature. Toluene was removed by roto-vac to obtain the nonionic vinyl surfactant monomer of Example 1.2.
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More