Additive composition
a technology of additive composition and composition, applied in the direction of lubricant composition, organic chemistry, fuel, etc., can solve the problems of increasing the downtime of the vehicle, increasing the wear of the lubricated engine components, and the inability to retain the basicity of the lubricant composition throughout its life, so as to improve the drain interval of engine oil
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example 1
Nominal 5 wt % Grafted E-P Rubber Dissolved in 300 TBN Sulfonate
[0037] Into a reaction flask equipped with a condenser, thermocouple, thermometer, gas inlet, and stirrer was added 500 gms of a 300 TBN sulfonate, H-611 manufactured by Afton Chemical (Richmond, Va.). The reagent was blanketed with nitrogen. The reaction was heated to 135° C. With vigorous stirring, 25 gms of an ethylene-propylene copolymer grafted with 1.99 wt % maleic anhydride, PA-1275 manufactured by DSM for Afton Chemical, was added to the reaction. The reaction was stirred for 6 hours or until the rubber was completely dissolved. Analyticals: TBN=294, Product exists as a semi-solid at room temperature.
example 2
Nominal 7.5 wt % Grafted E-P Rubber Dissolved in 300 TBN Sulfonate
[0038] Into a reaction flask equipped with a condenser, thermocouple, thermometer, gas inlet, and stirrer was added 500 gms of a 300 TBN sulfonate, H-611 manufactured by Afton Chemical (Richmond, Va.). The reagent was blanketed with nitrogen. The reaction was heated to 135° C. With vigorous stirring, 37.5 gms of an ethylene-propylene copolymer grafted with 1.99 wt % maleic anhydride, PA-1275 manufactured by DSM for Afton Chemical, was added to the reaction. The reaction was stirred for 6 hours or until the rubber was completely dissolved. Analyticals: TBN=290, Product solidified on cooling.
example 3
Nominal 10 wt % Grafted E-P Rubber Dissolved in 300 TBN Sulfonate
[0039] Into a reaction flask equipped with a condenser, thermocouple, thermometer, gas inlet, and stirrer was added 500 gms of a 300 TBN sulfonate, H-611 manufactured by Afton Chemical (Richmond, Va.). The reagent was blanketed with nitrogen. The reaction was heated to 135° C. With vigorous stirring, 50 gms of an ethylene-propylene copolymer grafted with 1.99 wt % maleic anhydride, PA-1275 manufactured by DSM for Afton Chemical, was added to the reaction. The reaction was stirred for 6 hours or until the rubber was completely dissolved. Analyticals: TBN=284, Product solidified on cooling.
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