Hydrometallurgical process for nickel oxide ore

a nickel oxide and hydrometallurgical technology, applied in the direction of nickel compounds, separation processes, solvent extraction, etc., can solve the problems of flash tank pressure-like impact, large discharged water, and inability to supply ore slurry as a raw material, so as to prevent inevitable operation shutdown and high operation efficiency

Inactive Publication Date: 2010-02-04
SUMITOMO METAL MINING CO LTD
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  • Abstract
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  • Claims
  • Application Information

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Benefits of technology

[0017]In view of the above conventional technological problems, it is an object of the present invention to provide a hydrometallurgical Process for a nickel oxide ore, which is capable of preventing inevitable operation shutdown of the above leaching step, and maintaining high operation efficiency as a whole process basis, in a hydrometallurgical Process for a nickel oxide ore, using...

Problems solved by technology

It should be noted that, at this stage, because temperature is still low and suitable operation condition has not been attained, the ore slurry as a raw material cannot be supplied.
That is, in the case where they are connected at a temperature of below 150° C., for example, use amount of industrial water to be supplied instead of the ore slurry increases, resulting in generation of a large amount of discharged water.
In this sense, it is desirable that they are connected at a temperature side as higher as possible near 180° C. However, in the case where they are connected at a temperature of over 180° C., for example, at equal to or higher than 200° C., difference between vapor pressure in the autoclave and vapor pressure in the flash tank becomes large, and thus pressure-like impact generates onto the flash tank in connection, and in the worst case, a valve or inner-lining brick of the flash tank are damaged.
In the former case, due to use of industrial water, discharged water generates in that amount, however, cooling rate is fast and thus temperature can be decreased in a shorter time.
In addition, in the latter case, although there is no discharged water generation, cooling rate is slow and thus a longer time is required in temperature decrease.
It should be not...

Method used

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  • Hydrometallurgical process for nickel oxide ore

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example 1

[0080]In the hydrometallurgical Process for a nickel oxide ore using the High Pressure Acid Leach, which process is shown in FIG. 1, countermeasures was prepared to take that, in the case of generation of a trouble of the steps other than the above leaching step, the leached slurry discharged from a three-stage flash tank, which configures the above High Pressure Acid Leach equipment of the leaching step, is subjected to self-circulation inside the High Pressure Acid Leach equipment, by transferring to the entrance side of a three-stage heater, which configures the above High Pressure Acid Leach equipment, as well as by shutdown of receiving the ore slurry and the addition of sulfuric acid to the autoclave, in the above leaching step. It should be noted that pH of the leached slurry to be self-circulated was controlled at 3.7, and temperature inside the autoclave at 220° C.

[0081]After one-year of operation performance (from January to December, 2007), the number of troubles generate...

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Abstract

The hydrometallurgical Process for a nickel oxide ore, which is capable of preventing inevitable operation shutdown of a leaching step and maintaining high operation efficiency as a whole process, in a trouble of the steps other than the leaching step, in a hydrometallurgical Process for a nickel oxide ore using a High Pressure Acid Leach.
It is characterized in that, the hydrometallurgical Process for a nickel oxide ore using a High Pressure Acid Leach equipment equipped with the following means (a) to (c), in a trouble of the steps other than the above leaching step, the leached slurry discharged from the means (c), which is used in the above High Pressure Acid Leach equipment, is subjected to self-circulation inside the High Pressure Acid Leach equipment, by transferring to the means (a), which is used in the above High Pressure Acid Leach equipment, as well as by shutdown of receiving the ore slurry and the addition of sulfuric acid, in the above leaching step:
  • means (a) to preliminarily increase temperature and pressure of the ore slurry;
  • means (b) to form the leached slurry, by the addition of sulfuric acid to the ore slurry with preliminarily increased temperature and pressure, and leaching under blow of high-pressure steam and high-pressure air;
  • means (c) to eliminate a pressurized state of the leached slurry formed.

Description

BACKGROUND OF THE INVENTION[0001]1. Field of the Invention[0002]The present invention relates to a hydrometallurgical Process for a nickel oxide ore, in more detail, in a hydrometallurgical Process for a nickel oxide ore using a High Pressure Acid Leach including a preparation step of ore slurry for making a slurry of a nickel oxide ore, a leaching step for obtaining leached slurry by transferring the relevant ore slurry to a High Pressure Acid Leach equipment for leaching nickel and cobalt, and a solid-liquid separation step of the relevant leached slurry, the present invention relates to a hydrometallurgical Process for a nickel oxide ore, which is capable of preventing inevitable operation shutdown of the above leaching step and maintaining high operation efficiency as a whole process basis, in a trouble of the steps other than the above leaching step.[0003]2. Description of the Prior Art[0004]A High Pressure Acid Leach using sulfuric acid has been noticed in recent years, as a w...

Claims

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Application Information

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IPC IPC(8): C01G53/00
CPCC01G53/11C22B15/0093C22B23/0461C22B23/043C22B23/0453C22B23/0407Y02P10/20
Inventor SHIBAYAMA, KEISUKENAKAI, OSAMUOZAKI, YOSHITOMO
Owner SUMITOMO METAL MINING CO LTD
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