Thermally Conductive Composition
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Example 1
Physical Treatment of Filler with Surface Area Modifying Agent
[0046]Two different methods of physically treating fillers with a surface area modifying agent have been described.
Example
Example 1A
Solution Method
[0047]Nine grams of Pluronic F38 (EO-PO block copolymers with —OH terminations, Mw=4700 g / mol, available from BASF) was dissolved into 200 mL of water. Into the Pluronic F38-water solution, 91 g of boron nitride fillers (PTX60, available from Momentive Performance Inc., OH) were dispersed. The water was then evaporated with constant stirring and vacuum overnight. The resultant dry powder weighed 100 g.
Example
Example 1B
Fluidization Method
[0048]Nine grams of Pluronic F38 (EO-PO block copolymers with —OH terminations, Mw=4700 g / mol, available from BASF) was dissolved into 45 mL of water. The Pluronic F38-water solution and 91 g of boron nitride fillers (PTX60) were placed in a fluid bed coater (Model MFL.01 by Vector Corporation, IA) to physically treat the fillers. The resultant dry powder weighed 100 g.
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