Biglycan variant polypeptides and methods of use
a polypeptide and variant technology, applied in the field of proteoglycans, can solve the problems of negative influence of biglycan on the m form and the m form, and achieve the effect of preventing or treating a disorder in the subject and low bone mass
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example 2
M- and D-rhBGN are Chemically Distinct
[0138]The M and D forms purified from CHO clone 57 HIC pool over two size exclusion columns were further analyzed by Capillary Electrophoresis (FIG. 3) was conducted using an Agilent Bioanalyzer 2100 and Agilent Protein 80 assay kit under non-reducing conditions according to manufacturer's protocols. The apparent molecular weight and mobility of D-rhBGN (65.5 kd, 31.00, respectively) was greater than that of M-rhBGN (60 kd, 30.44, respectively), indicating differential posttranslational modification of the two forms.
[0139]The M and D forms were characterized by N-linked oligosaccaride profiling analysis (FIG. 4). Approximately 250 μg of M- and D-rhBGN were digested into glycopeptides with trypsin at 37° C. overnight. The glycopeptides were purified with a C18 cartridge, eluted in sequential elutions of 20%, 40%, and 100% isopropanol, combined, and dried. N-glycans were released by enzymatic cleavage with PNGase F, and then purified of contaminan...
example 3
M-rhBGN is Highly Active in Bioassays
[0140]M-rhBGN purified from CHO clone 171 by two rounds of SEC was analyzed (FIG. 5) by an in-vitro bioassay for biglycan activity where the ability of biglycan to potentiate agrin-induced AChR clustering in cultured H2K myotubes is measured based on the method described in (Amenta et al., J. Neuroscience, 2012). M-rhBGN showed a robust and broad dose-response. Activity was observed in a 30-fold range of >50% of maximal activity between 0.016-0.512 μg / ml. (FIG. 5.)
example 4
D-rhBGN Shows Low Bioactivity
[0141]The SEC fractions containing D-rhBGN were analyzed by the bioassay describe above. As shown in FIG. 5, there was only low activity (<25% of maximal) across the entire concentration range tested (0.004-0.512 μg / ml).
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