Optical compensation membrane for liquid crystal display
A technology of optical compensation film and liquid crystal display, which is applied in the field of optical compensation film and can solve the problems of difficult preparation and the like
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Embodiment 1
[0071] The PVA samples of Example 1 were prepared by the following sequential steps:
[0072] (1). The preparation degree of polymerization is 2600 and the degree of saponification is 98mol% of PVA ester particles;
[0073] (2). At a temperature of 80°C to 95°C, add PVA ester grains to water to dissolve the ester grains;
[0074] (3). Add methanol to the solution of (2) until the ratio of methanol to water is about 1:5 (at this time, the solid content of PVA is 8-10%), and obtain the first solution;
[0075] (4). At a temperature of 40°C to 70°C, the crosslinking agent melamine formaldehyde (purchased from Cytec Company, product name cymel 303) and the catalyst p-toluenesulfonic acid are mixed and stirred for 15min to 1hr to obtain the second Solution (wherein, by weight, the consumption of cross-linking agent is 25wt% of PVA, and the consumption of catalyst is 6.25wt% of PVA);
[0076] (5). Add the second solution to the first solution and stir for 30min to 1hr to obtain a ...
Embodiment 2
[0098] In this example, the C plate prepared in Example 1 is used to make a TN-LCD, and the measured viewing angles are listed in Table 2, Figure 4 It is the equal contrast curve figure of embodiment 2.
[0099] Table 2
[0100]
Embodiment 3
[0102] Embodiment 3 is prepared in the same manner as Example 1, but the degree of polymerization of the PVA used in Embodiment 3 is respectively 3800, and the test results are also shown in Table 2, and the obtained equal contrast curves are as follows Figure 5 shown.
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