Method for proceeding Feituo Synthesizing reaction and catalyst specially for the same
一种催化剂、纳米催化剂的技术,应用在有机化合物/氢化物/配位配合物催化剂、物理/化学过程催化剂、催化反应等方向,能够解决总压力苛刻、产物分子量大等问题,达到好低温活性、广阔应用前景的效果
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Embodiment 1
[0023] 73mg RuCl 3 ·nH 2 O and 620mg of polyvinylpyrrolidone (polyvinylpyrrolidone: Ru=20, molar ratio, the same below) were added to 20ml of water, stirred and mixed, and then added to a 60ml autoclave at 150°C, 20atm H 2 The catalyst for the reaction was obtained by reducing it for 2 hours. The prepared ruthenium nanoparticles have an average particle size of 1.8±0.4nm, and the transmission electron micrographs and particle size distribution of the ruthenium nanoparticles are shown in Figure 1a and Figure 1b, respectively.
[0024] Cool the catalyst to room temperature, release residual gas, and then fill with 10atm CO, 20atm H 2 , react at 150°C. The reaction results are shown in Table 1.
Embodiment 2
[0026] 73mg RuCl 3 ·nH 2 O and 106mg of polyvinylpyrrolidone (polyvinylpyrrolidone: Ru=3.4) were added to 20ml of 1,4-dioxane, stirred and mixed, and then added to a 60ml autoclave at 150°C, 20atmH 2 The catalyst for the reaction was obtained by reducing it for 2 hours. Cool to room temperature, release residual gas, fill with 10atmCO, 20atmH 2 , react at 150°C. The reaction results are shown in Table 1.
Embodiment 3
[0028] 73mg RuCl 3 ·nH 2 O and 106mg of polyvinylpyrrolidone (polyvinylpyrrolidone: Ru=3.4) were added to 20ml of ethanol, stirred and mixed, and then added to a 60ml autoclave at 150°C, 20atmH 2 The catalyst for the reaction was obtained by reducing it for 2 hours. Cool to room temperature, release residual gas, fill with 10atm CO, 20atm H 2 , react at 150°C. The reaction results are shown in Table 1.
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