A new pulp and process for pulping
A technology of pulp and tetraalkylammonium salt, applied in the fields of lignocellulosic materials, pulping methods of lignocellulosic materials and softening of lignocellulosic materials, can solve the problems of low carbohydrate yield organic sulfur compounds, etc.
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Embodiment 1
[0094] Treat cork in 40% aqueous tetrabutylammonium hydroxide at 170 °C for 5 min in a microwave field
[0095] In a sealed reactor tube equipped with a magnetic stirring bar, about 750 mg of cork sticks were mixed in 4,5 ml of 40% tetrabutylammonium hydroxide in water and stirred at 170° C. for 5 minutes.
[0096] Stirring resulted in a dark brown solution containing long nits. Washing with water gave two separate bundles of light beige fibers as well as completely separated fibers.
Embodiment 2
[0098] Treat cork in 20% aqueous tetrabutylammonium hydroxide at 170°C for 5 minutes in a microwave field
[0099] In a sealed reactor tube equipped with a magnetic stirring bar, about 750 mg of cork sticks were mixed in 4,5 ml of 20% tetrabutylammonium hydroxide in water and stirred at 170° C. for 5 minutes.
[0100] Stirring resulted in a dark brown solution containing long nits. Washing with water gave two separate bundles of light beige fibers as well as completely separated fibers. The pulp composition is slightly more complete than Example 1.
Embodiment 3
[0102] Treat cork in 10% aqueous tetrabutylammonium hydroxide at 170°C for 5 minutes in a microwave field
[0103] In a sealed reactor tube equipped with a magnetic stirring bar, about 750 mg of a cork stick were mixed in 4,5 ml of a 10% aqueous solution of tetrabutylammonium hydroxide and stirred at 170° C. for 5 minutes.
[0104] Stirring resulted in a dark brown solution containing long nits. Washing with water gave two separate bundles of light beige fibers with a more complete pulp composition than Example 2.
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