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Method of treating fire retardant wood using microwave

A microwave treatment and wood technology, applied in wood treatment, wood impregnation, wood impregnation, etc., can solve problems such as restricting wood drying speed, carbonization, outer coke and inner drying, etc., to solve a large number of enrichment and serious segregation, and improve distribution conditions. , the effect of improving permeability

Inactive Publication Date: 2008-11-19
KUNMING UNIV OF SCI & TECH
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  • Claims
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AI Technical Summary

Problems solved by technology

Since wood is a poor conductor of heat, especially in the stage of low moisture content, its thermal conductivity is very low, which seriously restricts the improvement of wood drying speed.
Most of the wood drying methods in the prior art have the following problems: (1) the drying cycle is long, generally 6 to 24 hours, and the drying time of individual thicker wood is longer; (2) drying is uneven, often showing as wood surface Drying and internal humidity seriously affect the dimensional stability and mechanical properties of wood; (3) The drying efficiency is low, because most of them are intermittent dry operations, so the labor intensity is high
The main problems of the traditional method in the flame retardant treatment of wood are: (A) the drying rate is low, which is easy to cause the flame retardant treatment period of the wood to be long (the cycle of large size and high thickness wood is longer); (B) the drying is uneven, resulting in " The phenomenon of "dry on the outside and wet on the inside" will reduce the anti-corrosion performance of the wood, or increase the drying time to cause the phenomenon of "coke on the outside and dry on the inside", and even cause the surface of the wood to crack, darken the color, or even carbonize, seriously affecting the appearance and quality of the wood. Mechanical properties; (C) During the drying process of wood, the liquid containing flame retardant diffuses outwards through the traditional seepage method, causing the solute of the flame retardant to continuously migrate outwards, enriching in a large amount on the surface of the wood, and making the flame retardant The distribution in the wood is seriously uneven, and severe segregation occurs, which directly affects the flame retardant performance of the wood, and at the same time affects the properties of the wood surface and subsequent processing performance. Since the content of the fire retardant in the wood core is very small, it will , once the wood surface is damaged, the wood immediately loses its flame retardant properties, causing huge losses to production and life

Method used

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  • Method of treating fire retardant wood using microwave

Examples

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Effect test

Embodiment 1

[0021] A. The oak with a size of 1500mm × 200m × 25mm and an initial moisture content of 30% is sent to a microwave processing device with a microwave frequency of 915MHz. Under normal pressure, the drying temperature is controlled at 60°C and dried for 10 minutes. It is dried to a moisture content of 10%; B, the dried wood in step A is sent to a vacuum pressurized tank, vacuumed to a vacuum degree of 77KPa, and the vacuum is released, and a mixed solution is compounded with an inorganic flame retardant in the following mass ratio: 20 % ureidophosphate, 10% boric acid, 70% water, under the gauge pressure of 1.6MPa, soak the wood for 15 minutes, release the pressure, discharge the flame retardant, and then vacuumize to 77KPa vacuum degree, release the vacuum , and then take out the wood; C. Send the wood in step B to a microwave treatment device with a microwave frequency of 915MHz, and under normal pressure, control the drying temperature at 60°C and dry for 3 minutes to obtain...

Embodiment 2

[0023]A, the size is 300mm * 100m * 25mm, the Changbai larch with initial moisture content of 42%, is sent in the microwave treatment device that microwave frequency is 2450MHz, under normal pressure, control drying temperature 80 ℃, dry 10 minutes, namely It can be dried to a moisture content of 8%; B. Send the above-mentioned wood to a vacuum pressurized tank, evacuate to a vacuum of 77KPa, release the vacuum, and compound the mixed solution with the following mass ratio of inorganic flame retardant: 15% Dirukon's FRT in the United States, 12% borax, 73% water, soak the wood for 30 minutes under a gauge pressure of 1.2MPa, release the pressure, discharge the flame retardant, and then vacuumize to 77KPa vacuum degree, release the vacuum , and then take out the wood; C. Send the above wood to a microwave treatment device. Under normal pressure, the drying temperature is controlled at 80°C, and the drying time is 2 minutes to obtain a flame-retardant dry Changbai larch board wit...

Embodiment 3

[0025] A. Put the masson pine with a size of 200mm×100m×60mm and an initial moisture content of 52% into a microwave dryer with a microwave frequency of 2450MHz. Under normal pressure, the drying temperature is controlled at 70°C and dried for 10 minutes. It is dried to a moisture content of 12%; B, the wood is sent to a vacuum pressurized tank, vacuumed to a vacuum degree of 377KPa, and the vacuum is removed, and the mixed solution is compounded with the following mass ratio of inorganic flame retardants: 18% poly Ammonium phosphate APP, 6% ammonium pentaborate, 76% water, under the gauge pressure of 1.4MPa, soak the wood for 25 minutes, release the pressure, discharge the flame retardant, and then vacuumize to 57KPa vacuum degree, release the vacuum, Then take out the wood; C, send the above-mentioned wood to the microwave treatment device, under normal pressure, the drying temperature is controlled at 75°C, and drying for 3 minutes can obtain the flame-retardant dried masson...

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Abstract

The invention provides a method for processing fire retarding wood with microwave. The method comprises the following steps: heating and processing wood through microwave; subjecting to vacuum pressure treatment; soaking the wood in flame retardant solution with mass ratio being 5-50% and under the atmospheric pressure of 0.1-10MPa for 3-720 minutes; subjecting to vacuum pressure treatment; and heating and treating through microwave to obtain the fire retarding wood. Since heat is not conducted from the outer part of the wood, but in the wood through the interaction between the microwave alternative electric field and water molecules, so as to quickly raise the whole temperature of the wood and improve the permeability of the heat, and meanwhile, kill bristletails and ova in the wood, improve the distribution state of flame retardant in the wood, and enable the flame retardant not to be segregated in-situ along with the migration of the solution, thus basically solving the problems with the traditional method that the flame retardant is present in large amounts on the surface of the wood and serious segregation occurs to the flame retardant when the fire retarding wood is treated. In addition to microwave heating, no additional heat energy is consumed. The fire retarding wood can be directly used as architectural decorative materials.

Description

technical field [0001] The invention relates to a method for treating flame-retardant wood, specifically a method for treating flame-retardant wood with microwave drying technology, and belongs to the technical field of wood processing. Background technique [0002] The flame retardancy of wood depends not only on the performance and dosage of flame retardants, but also on the distribution of flame retardants inside the wood. The main indicator affecting the penetration of flame retardants in wood is the fluid permeability of wood. The fluid permeability of wood is a physical quantity describing the difficulty of fluid penetration in wood. Since the penetration of fluid in wood is different from the diffusion of fluid in wood, in the process of wood treatment, the drainage of water and the infusion of liquid are both Closely related to the permeability of wood. Therefore, in order to ensure that the flame retardant can fully penetrate into the wood and form an effective dr...

Claims

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Application Information

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IPC IPC(8): B27K5/04B27K3/08B27K3/32
Inventor 陈冬华郭玉忠刘应杰
Owner KUNMING UNIV OF SCI & TECH
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